1-甲基-5-巯基-1H-四氮唑合成路线 （共 24 条）
反应条件
pyridine; methanol 1.) freon TF, CH2Cl2, from 0 to 5 deg C, 30 min, 2.) from 0 to 5 deg, 10 min; Yield given. Multistep reaction;
参考文献
Walker, Donald G.; Brodfuehrer, Paul R.; Brundidge, Steven P.; Shih, Kun Mao; Sapino, Chester
Journal of Organic Chemistry, 1988 , vol. 53, # 5 p. 983 - 991
反应条件
pyridine; methanol 1.) CH2Cl2, 2.) from 0 to 5 deg C, 15 min; Yield given. Multistep reaction;
参考文献
Walker, Donald G.; Brodfuehrer, Paul R.; Brundidge, Steven P.; Shih, Kun Mao; Sapino, Chester
Journal of Organic Chemistry, 1988 , vol. 53, # 5 p. 983 - 991
反应条件
in various solvent(s) T=-263.15°C; UV-irradiation; Product distribution;
参考文献
Gomez-Zavaglia, A.; Reva, I. D.; Frija, L.; Cristiano, M. L.; Fausto, R.
Journal of Molecular Structure, 2006 , vol. 786, # 2-3 SP p. 182 - 192
反应条件
dihydrogen peroxide
bei Siedetemperatur;
参考文献
Stolle; Henke-Stark
Journal fuer Praktische Chemie (Leipzig), 1929 , vol. <2>124, p. 275
参考文献
Stolle; Henke-Stark
Journal fuer Praktische Chemie (Leipzig), 1929 , vol. <2>124, p. 275
反应条件
sodium hydroxide; tetrabutylammomium bromide in chloroform
T=20°C; Methylation; 5 h;
参考文献
Gol'tsberg; Koldobskii
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 8 p. 1194 - 1201
反应条件
potassium carbonate in water; acetone
参考文献
Otsuka Pharmaceutical Company, Limited
Patent: US4540703 A1, 1985 ;
反应条件
potassium carbonate in acetone
4 h; Heating;
参考文献
Uchida; Komatsu; Morita; Kanbe; Nakagawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 2 p. 322 - 326
反应条件
potassium carbonate in acetone
3 h; Heating;
参考文献
Uchida; Komatsu; Morita; Kanbe; Yamasaki; Nakagawa
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 4 p. 958 - 961
反应条件
potassium carbonate in dichloromethane
24 h; Heating;
参考文献
Quast, Helmut; Nahr, Uwe
Chemische Berichte, 1983 , vol. 116, # 10 p. 3427 - 3437
