8-甲氧基-Alpha-四氢萘酮合成路线 （共 17 条）
反应条件
palladium 10 on activated carbon; hydrogen in ethanol T=20°C; 24 h;
参考文献
Cabrera, Elvia V.; Banerjee, Ajoy K.
Organic Preparations and Procedures International, 2010 , vol. 42, # 5 p. 499 - 502
反应条件
potassium carbonate in acetone 30 h; Heating;
参考文献
Bilger, Christine; Demerseman, Pierre; Royer, Rene
European Journal of Medicinal Chemistry, 1987 , vol. 22, p. 363 - 365
反应条件
potassium phosphate in dimethyl sulfoxide T=60°C; 0.333333 h;
参考文献
Sharshira, Essam Mohamed; Iwanami, Haruki; Okamura, Mutsuo; Hasegawa, Eietsu; Horaguchi, Takaaki
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 1 p. 17 - 25
反应条件
1: 2-Methoxy-6-methylbenzoic acid ethyl ester With lithium diisopropyl amide in tetrahydrofuran T=-78°C; 0.25 h; 2: acrylic acid methyl ester in tetrahydrofuran T=0°C; 5 h; Further stages.;
参考文献
Yang, Rui-Yang; Kizer, Darin; Wu, Hui; Volckova, Erika; Miao, Xiu-Sheng; Ali, Syed M.; Tandon, Manish; Savage, Ronald E.; Chan, Thomas C.K.; Ashwell, Mark A.
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 10 p. 5635 - 5643
反应条件
1: 1.) Bu3N, Pd(OAc)2, 2.) H2 / 2.) 10percent Pd/C / 1.) 100 deg C, 9 h, 2.) MeOH, 50 psi, 5 h 2: 6 N aq. KOH / ethanol / 2 h / Heating 3: polyphosphoric ester / CHCl3 / 7 h / Ambient temperature View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 29, # 4 p. 477 - 480
反应条件
sodium iodide; zinc in ethylene glycol dimethyl ether 8 h; Reflux;
参考文献
Banerjee, Ajoy K.; Bedoya, Liadis; Adherian, Maria E.; Vera, William J.; Cabrera, Elvia V.; Kariney, Elidig R.
Journal of Chemical Research, 2010 , # 9 p. 522 - 524
反应条件
1: 61 percent / Br2 / CHCl3 / 0.5 h / 5 °C 2: 94 percent / polyphosphoric acid / 1 h / Heating 3: 65 percent / H2, triethylamine View Scheme
参考文献
Tetrahedron, , vol. 36, # 17-K p. 2513 - 2520
反应条件
1: 6 N aq. KOH / ethanol / 2 h / Heating 2: polyphosphoric ester / CHCl3 / 7 h / Ambient temperature View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 29, # 4 p. 477 - 480
反应条件
polyphosphoric ester in chloroform 7 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Organic Preparations and Procedures International, , vol. 29, # 4 p. 477 - 480
反应条件
1: 94 percent / polyphosphoric acid / 1 h / Heating 2: 65 percent / H2, triethylamine View Scheme
参考文献
Tetrahedron, , vol. 36, # 17-K p. 2513 - 2520
