alpha-酮戊二酸二甲酯合成路线 （共 32 条）
反应条件
boron trifluoride T=65°C; 0.333333 h;
参考文献
Jaoui; Kleindienst; Lewandowski; Edney
Analytical Chemistry, 2004 , vol. 76, # 16 p. 4765 - 4778
反应条件
in diethyl ether T=0°C; 4 h;
参考文献
Hagen, Timothy J.; Narayanan, Krishnaswamy; Names, Jeffrey; Cook, James M.
Journal of Organic Chemistry, 1989 , vol. 54, # 9 p. 2170 - 2178
反应条件
1: 30 percent / H2 / Pd/C / methanol / 48 h 2: 1.) Ozon; 2.) HCl / 1.) methylenechlorid, -60 deg C; 2.) methanol, room temp, 90 min. View Scheme
参考文献
Tetrahedron, , vol. 37, # 1 p. 105 - 112
反应条件
in methanol; benzene 0.5 h; Ambient temperature;
参考文献
Mashimoto, Norio; Aoyama, Toyohiko; Shioiri, Takayuki
Chemical & Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1475 - 1478
反应条件
hydrogenchloride T=90°C; Erwaermen des Reaktionsprodukts mit Schwefelsaeure enthaltendem Methanol.;
参考文献
Technology Reports of the Osaka University, , vol. 7, p. 177,182
Kogyo Kagaku Zasshi, , vol. 58, p. 806
Technology Reports of the Osaka University, , vol. 7, p. 177,181
反应条件
o-MeO-2-nitrostyrene; tin(IV) chloride other reagents: boron trifluoride etherate/2-methoxy-β-nitrostyrene, benzaldehyde, benzaldehyde, benzaldehyde dimethyl acetal;
参考文献
Tetrahedron, , vol. 55, # 4 p. 943 - 954
反应条件
hydrogenchloride; ozone 1.) methylenechlorid, -60 deg C; 2.) methanol, room temp, 90 min.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 37, # 1 p. 105 - 112
反应条件
2,2-dimethoxy-propane 144 h; Ambient temperature;
参考文献
Journal fuer Praktische Chemie/Chemiker-Zeitung, , vol. 335, # 2 p. 176 - 180
反应条件
1: sulfuric acid / Electrolysis 2: aqueous hydrochloric acid , 35 percent / 90 °C / Erwaermen des Reaktionsprodukts mit Schwefelsaeure enthaltendem Methanol. View Scheme
参考文献
Technology Reports of the Osaka University, , vol. 7, p. 177,182
反应条件
Erwaermen des Reaktionsprodukts mit Methanol und wenig Schwefelsaeure;
参考文献
Technology Reports of the Osaka University, , vol. 7, p. 177,182
