2-苯基-1-(噻吩-2-基)乙酮合成路线 （共 22 条）
反应条件
tin(IV) chloride in benzene T=30°C; Friedel-Crafts acylation; 3 h;
参考文献
Parella, Ramarao; Naveen; Kumar, Amit; Babu, Srinivasarao Arulananda
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1738 - 1742
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; copper diacetate in water; acetonitrile T=20°C; 6 h; Green chemistry;
参考文献
Jiang, Jian-An; Du, Jia-Lei; Wang, Zhan-Guo; Zhang, Zhong-Nan; Xu, Xi; Zheng, Gan-Lin; Ji, Ya-Fei
Tetrahedron Letters, 2014 , vol. 55, # 10 p. 1677 - 1681
反应条件
potassium hexamethylsilazane; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran 0.75 h; Heating;
参考文献
Hamann, Blake C.; Hartwjg, John F.
Journal of the American Chemical Society, 1997 , vol. 119, # 50 p. 12382 - 12383
反应条件
P2O5 in thiophene; dichloromethane
参考文献
Katritzky, Alan R.; Suzuki, Kazuyuki; Singh, Sandeep K.
Croatica Chemica Acta, 2004 , vol. 77, # 1-2 p. 175 - 178
反应条件
PPA T=60 - 80°C; Acylation; Friedel-Crafts acylation; 2 h;
参考文献
Renault, Olivier; Dallemagne, Patrick; Rault, Sylvain
Organic Preparations and Procedures International, 1999 , vol. 31, # 3 p. 324 - 328
反应条件
zinc dibromide in dichloromethane T=90°C; 12 h;
参考文献
Katritzky, Alan R.; Suzuki, Kazuyuki; Singh, Sandeep K.
Croatica Chemica Acta, 2004 , vol. 77, # 1-2 p. 175 - 178
反应条件
silica gel supported sodium carbonate in chlorobenzene T=135°C; 6 h;
参考文献
Aoyama, Tadashi; Orito, Mami; Takido, Toshio; Kodomari, Mitsuo
Synthesis, 2008 , # 13 p. 2089 - 2099
反应条件
palladium(II) dichloride bis[bis(diphenylphosphine)ferrocene] dichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide T=100°C; Stille coupling; 16 h;
参考文献
Saevmarker, Jonas; Lindh, Jonas; Nilsson, Peter
Tetrahedron Letters, 2010 , vol. 51, # 52 p. 6886 - 6889
反应条件
PPA T=60 - 80°C; Acylation; Friedel-Crafts acylation; 2 h;
参考文献
Renault, Olivier; Dallemagne, Patrick; Rault, Sylvain
Organic Preparations and Procedures International, 1999 , vol. 31, # 3 p. 324 - 328
反应条件
potassium tert-butylate in dimethyl sulfoxide T=40°C; 3 h; Irradiation;
参考文献
Baumgartner, Maria T.; Gallego, Mariana H.; Pierini, Adriana B.
Journal of Organic Chemistry, 1998 , vol. 63, # 18 p. 6394 - 6397
