2,3-O-异亚丙基-D-呋喃核糖苷合成路线 (共 4 条)
参考文献
Behr, Jean-Bernard
Tetrahedron Letters, 2009 , vol. 50, # 31 p. 4498 - 4501
反应条件
1H-imidazole in dichloromethane T=20°C; 3 h;
参考文献
Yadav, Jhillu S.; Nageshwar Rao, Ragam; Somaiah, Ragam; Harikrishna, Valaboju; Subba Reddy, Basi V.
Helvetica Chimica Acta, 2010 , vol. 93, # 7 p. 1362 - 1368
反应条件
1: 2,3-O-Isopropylidene-D-ribose With 1H-imidazole in dichloromethane T=0°C; 0.5 h; Inert atmosphere; 2: tert-butylchlorodiphenylsilane in dichloromethane T=20°C; 8 h; Inert atmosphere;
参考文献
Srihari; Sathish Reddy; Yadav; Yedlapudi; Kalivendi, Shasi V.
Tetrahedron Letters, 2013 , vol. 54, # 41 p. 5616 - 5618
反应条件
1: 2,3-O-Isopropylidene-D-ribose With 1H-imidazole in dichloromethane
T=0°C; 0.5 h; Inert atmosphere;
2: tert-butylchlorodiphenylsilane in dichloromethane
T=20°C; 8 h; Inert atmosphere;
参考文献
Srihari; Sathish Reddy; Yadav; Yedlapudi; Kalivendi, Shasi V.
Tetrahedron Letters, 2013 , vol. 54, # 41 p. 5616 - 5618