2-(甲基氨基)乙酸乙酯合成路线 （共 47 条）
参考文献
Jankowski,K.; Berse,C.
Canadian Journal of Chemistry, 1968 , vol. 46, p. 1939 - 1942
反应条件
triethylamine in tetrahydrofuran; diethyl ether
参考文献
Dr. Karl Thomae GmbH
Patent: US4550107 A1, 1985 ;
US 4550107 A
反应条件
water; hydrazine hydrate
参考文献
Barnett; Morris
Biochemical Journal, 1946 , vol. 40, p. 450,451
反应条件
tributyl-amine; Pd(OAc)2*PPh3 in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=110°C; P=2280 Torr; 72 h;
参考文献
Mori, Miwako; Kimura, Masaya; Uozumi, Yasuhiro; Ban, Yoshio
Tetrahedron Letters, 1985 , vol. 26, # 48 p. 5947 - 5950
反应条件
tributyl-amine; Pd(OAc)2*PPh3 in xylene
T=110°C; P=2280 Torr; 72 h;
参考文献
Mori, Miwako; Kimura, Masaya; Uozumi, Yasuhiro; Ban, Yoshio
Tetrahedron Letters, 1985 , vol. 26, # 48 p. 5947 - 5950
反应条件
diethyl ether
anschliessende Cyclisierung mit Hilfe von wss.-aethanol. HCl bzw. wss. HCl;
参考文献
Elmore
Journal of the Chemical Society, 1958 , p. 3489,3492
反应条件
(i) ClCO2Et, Et3N, (ii) /BRN= 1700745/, (iii) KOH; Multistep reaction;
参考文献
Byk Gulden Lomberg
Patent: DE2856753 , 1979 ;
Chem.Abstr., 1979 , vol. 91, # 175033
反应条件
(i) ClCO2Et, Et3N, (ii) /BRN= 1700745/, (iii) KOH; Multistep reaction;
参考文献
Byk Gulden Lomberg
Patent: DE2856753 , 1979 ;
Chem.Abstr., 1979 , vol. 91, # 175033
反应条件
hydrogenchloride in ethanol
18 h; Heating;
参考文献
Agababyan, A. G.; Gevorgyan, G. A.; Tumadzhyan, A. E.; Melkonyan, Zh. S.; Durgaryan, L. K.; et al.
Pharmaceutical Chemistry Journal, 1983 , vol. 17, # 3 p. 195 - 200
Khimiko-Farmatsevticheskii Zhurnal, 1983 , vol. 17, # 3 p. 303 - 308
反应条件
hydrogenchloride; triethylamine in dichloromethane
T=20°C; 0.5 h;
参考文献
Societe de Conseils de Recherches et d'Applications Scientifiques (S.C.R.A.S.)
Patent: US6335445 B1, 2002 ;
Location in patent: Page column 93-94 ;
