甲基(1R)-3-氧代环戊烷羧酸酯合成路线 (共 4 条)
反应条件
(2S,5S)-5-benzyl-3-methyl-2-(5-methyl-furan-2-yl)-imidazolidin-4-one; trichloroacetic acid in diethyl ether T=-10°C; 1 h; Title compound not separated from byproducts.;
参考文献
Tuttle, Jamison B.; Ouellet, Stephane G.; MacMillan, David W. C.
Journal of the American Chemical Society, 2006 , vol. 128, # 39 p. 12662 - 12663
反应条件
cation exchange resin 24 h; Heating;
参考文献
Sung, Sun-Young; Frahm, August Wilhelm
Archiv der Pharmazie, 1996 , vol. 329, # 6 p. 291 - 300
反应条件
glucose dehydrogenase; D-glucose; enoate-reductase YQJm from Bacillus subtilis mutant I69T; nicotinamide adenine dinucleotide phosphate T=30°C; pH=7; aq. phosphate bufferEnzymatic reaction; optical yield given as percent ee;
参考文献
Bougioukou, J. Despina; Kille, Sabrina; Taglieber, Andreas; Reetz, Manfredt.
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 18 p. 3287 - 3305
反应条件
2: 98 percent / cation exchange resin / 24 h / Heating View Scheme
参考文献
Sung, Sun-Young; Frahm, August Wilhelm
Archiv der Pharmazie, 1996 , vol. 329, # 6 p. 291 - 300