1,3-二(2-氯苯基)脲合成路线 （共 29 条）
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; caesium carbonate; (9,9-dimethyl-9H-xanthene-4,5-diyl)bis(bis(3,5-bis(trifluoromethyl)phenyl)phosphine) in 1,4-dioxane
T=100°C; 5 h;
参考文献
Sergeev, Alexey G.; Artamkina, Galina A.; Beletskaya, Irina P.
Tetrahedron Letters, 2003 , vol. 44, # 25 p. 4719 - 4723
反应条件
triethylamine in dichloromethane
T=0 - 20°C;
参考文献
Clayden, Jonathan; Lemiegre, Loic; Pickworth, Mark; Jones, Lyn
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 16 p. 2908 - 2913
反应条件
1,2,4,5-tetramethyl benzene; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in 1,4-dioxane
T=100°C; 11 h;
参考文献
Sergeev; Artamkina; Beletskaya
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 12 p. 1741 - 1752
反应条件
zirconium oxide; molybdenum in 1,2-dichloro-benzene
T=69.85°C; Condensation; 6 h;
参考文献
Reddy, Benjaram M.; Reddy, Vangala R.
Synthetic Communications, 1999 , vol. 29, # 16 p. 2789 - 2794
反应条件
PEG-400; cerium(III) chloride; potassium iodide in water
0.266667 h; microwave irradiation;
参考文献
Li, Zheng
Synthetic Communications, 2005 , vol. 35, # 17 p. 2325 - 2331
反应条件
copper diacetate; palladium diacetate in 1,4-dioxane
P=760.051 Torr; Reflux;
参考文献
Guan, Zheng-Hui; Lei, Hao; Chen, Ming; Ren, Zhi-Hui; Bai, Yinjuan; Wang, Yao-Yu
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 489 - 496
反应条件
1,10-phenanthroline; Pd(1,10-phenanthroline)2(OTf)2
T=135°C; P=45003.6 Torr; 2 h;
参考文献
Wchman, Petra; Borst, Leo; Kamer, Paul C. J.; Van Leeuwen, Piet W. N. M.
Chemische Berichte, 1997 , vol. 130, # 1 p. 13 - 21
参考文献
Dyer; McCormick
Journal of the American Chemical Society, 1946 , vol. 68, p. 986
反应条件
in acetonitrile
1.5 h; Heating;
参考文献
Arrieta, Ana; Palomo, Claudio
Tetrahedron Letters, 1981 , vol. 22, # 18 p. 1729 - 1732
反应条件
ethanol
0.0166667 h; Microwave irradiationNeat (no solvent);
参考文献
Uberhande; Thakare; Berad
Journal of the Indian Chemical Society, 2010 , vol. 87, # 9 p. 1137 - 1141
