6-S-(4-氯苯基)-6-硫代-肌苷合成路线 （共 1 条）
反应条件
1: 84 percent / toluene-4-sulphonic acid monohydrate / tetrahydrofuran / 1 h / 50 °C
2: 88 percent / 3-chloroperbenzoic acid / CH2Cl2 / 2.5 h / -5 °C
3: 70 percent / N,N-di-isopropylethylamine / N,N-dimethyl-acetamide / 28 h / 70 - 75 °C
4: 0.65 g / aq. formic acid / 3 h / Ambient temperature
5: hydrogen / palladium on carbon / ethanol; acetic acid; H2O / 2 h
View Scheme
参考文献
Buck, Ildiko M.; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 2937 - 2942
