1: 2-propenylmagnesium bromide With manganese (II) chloride in tetrahydrofuran Metallation; 2: α,α,α',α'-tetrabromo-o-xylene in tetrahydrofuran T=0°C; Substitution; 2.5 h; 3: With water Substitution;
参考文献
Kakiya; Shinokubo; Oshima
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 9 p. 2139 - 2147
sodium iodide in N,N-dimethyl-formamide T=70 - 80°C; 10 h;
参考文献
Kopranenkov, V. N.; Vorotnikov, A. M.; Dashkevich, S. N.; Luk'yanets, E. A.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 4 p. 900 - 906,803 - 809
