(2-氨基苯基)(苯基)甲醇合成路线 (共 39 条)
反应条件
1: CuCl2*H2O; potassium carbonate / N,N-dimethyl-formamide / 24 h / 60 °C
2: tert.-butylhydroperoxide; iodine / isobutyramide; water / 24 h / 120 °C / Sealed tube
View Scheme
参考文献
Yan, Yizhe; Wang, Zhiyong
Chemical Communications, 2011 , vol. 47, # 33 p. 9513 - 9515
反应条件
potassium hydroxide in poly(ethylene glycol)-400
T=80°C;
参考文献
Wu, Fang-Wen; Hou, Rei-Sheu; Wang, Huey-Min; Kang, Iou-Jiun; Chen, Ling-Ching
Journal of the Chinese Chemical Society, 2012 , vol. 59, # 4 p. 535 - 539
反应条件
potassium hydroxide in poly(ethylene glycol)-400
T=80°C;
参考文献
Wu, Fang-Wen; Hou, Rei-Sheu; Wang, Huey-Min; Kang, Iou-Jiun; Chen, Ling-Ching
Journal of the Chinese Chemical Society, 2012 , vol. 59, # 4 p. 535 - 539
反应条件
toluene-4-sulfonic acid in toluene
2 h; Heating;
参考文献
Aritomi, Jiro; Ueda, Shozo; Nishimura, Haruki
Chemical & Pharmaceutical Bulletin, 1981 , vol. 29, # 12 p. 3712 - 3715
反应条件
1: CuCl2*H2O; potassium carbonate / N,N-dimethyl-formamide / 24 h / 60 °C
2: tert.-butylhydroperoxide; iodine / isobutyramide; water / 24 h / 120 °C / Sealed tube
View Scheme
参考文献
Yan, Yizhe; Wang, Zhiyong
Chemical Communications, 2011 , vol. 47, # 33 p. 9513 - 9515
反应条件
1: CuCl2*H2O; potassium carbonate / N,N-dimethyl-formamide / 24 h / 60 °C
2: tert.-butylhydroperoxide; iodine / diethyl ether / 18 h / 80 °C
View Scheme
参考文献
Yan, Yizhe; Wang, Zhiyong
Chemical Communications, 2011 , vol. 47, # 33 p. 9513 - 9515
反应条件
hydrogenchloride in ethanol
T=65 - 70°C; 2 h; Yield given;
参考文献
Xu, Daqiang; Mattner, Paul G.; Kucerovy, Andrew; Prasad, Kapa; Repic, Oljan
Tetrahedron Asymmetry, 1996 , vol. 7, # 3 p. 747 - 754
参考文献
Gabriel; Stelzner
Chemische Berichte, 1896 , vol. 29, p. 1313
反应条件
CaO
T=560°C; 0.666667 h;
参考文献
Horaguchi, Takaaki; Oyanagi, Takako; Creencia, Evelyn Cuevas; Tanemura, Kiyoshi; Suzuki, Tsuneo
Journal of Heterocyclic Chemistry, 2004 , vol. 41, # 1 p. 1 - 6