1H-苯并[d][1,3]噁嗪-2(4h)-酮合成路线 (共 19 条)
反应条件
in toluene T=120°C; 12 h;
参考文献
Molina; Arques
Synthesis, 1991 , # 1 p. 21 - 23
反应条件
triethylamine in tetrahydrofuran 2 h; Ambient temperature;
参考文献
Uchida; Chihiro; Morita; Yamashita; Yamasaki; K anbe; Yabuuchi; Nakagawa
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 6 p. 1575 - 1586
反应条件
[bis(acetoxy)iodo]benzene in acetic acid 48 h; Ambient temperature;
参考文献
Beckwith, Athelstan L. J.; Dyall, Leonard K.
Australian Journal of Chemistry, 1990 , vol. 43, # 3 p. 451 - 461
反应条件
1: pyridine / acetonitrile / 1.) r.t., 12 h, 2.) reflux, 2 h 2: DBU / toluene / 1.5 h / Heating View Scheme
参考文献
Ren, Long; Jiao, Ning
Chemical Communications, 2014 , vol. 50, # 28 p. 3706 - 3709
反应条件
tri-ruthenium(0)dodecacarbonyl; tetraethylammonium chloride in various solvent(s) T=170°C; P=45600 Torr; 1 h; other Pd catalyst; other cocatalyst; var. solvents, reaction time, pressure and temperatures; also substituted benzyl alcohols; Product distribution;
参考文献
Cenini, S.; Console, S.; Crotti, C.; Tollari, S.
Journal of Organometallic Chemistry, 1993 , vol. 451, # 1.2 p. 157 - 162
反应条件
n-butyllithium in tetrahydrofuran; hexane 1.) -70 deg C, 2.) r.t.;
参考文献
Consonni, Roberto; Dalla Croce, Piero; Ferraccioli, Raffaella; La Rosa, Concetta
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 15 p. 1809 - 1814
反应条件
1: 85 percent / CH2Cl2 / 16 h / Ambient temperature 2: 74 percent / toluene / 12 h / 120 °C View Scheme
参考文献
Molina; Arques
Synthesis, 1991 , # 1 p. 21 - 23
参考文献
Kitamura
Yakugaku Zasshi, 1937 , vol. 57, p. 233,236, 239; dtsch. Ref. S. 58, 61
Chem.Abstr., 1937 , p. 4924
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Kitamura
Yakugaku Zasshi, 1934 , vol. 54, p. 98,102, 111; dtsch. Ref. S. 11, 16, 17
Chem.Abstr., 1936 , p. 3434
参考文献
Lindemann; Schultheis
Justus Liebigs Annalen der Chemie, 1928 , vol. 464, p. 246