4-氯 3-碘-苯甲酸甲酯合成路线 （共 6 条）
反应条件
Inert atmosphereReflux;
参考文献
Guo, Shengmei; Qian, Bo; Xie, Yinjun; Xia, Chungu; Huang, Hanmin
Organic Letters, 2011 , vol. 13, # 3 p. 522 - 525
反应条件
C27H37ClCuN3; potassium tert-butylate in tetrahydrofuran T=80°C; P=760.051 Torr; 8 h; Inert atmospheresealed tube;
参考文献
Inomata, Hiroshi; Ogata, Kenichi; Fukuzawa, Shin-Ichi; Hou, Zhaomin
Organic Letters, 2012 , vol. 14, # 15 p. 3986 - 3989
反应条件
potassium phosphate; bis-triphenylphosphine-palladium(II) chloride in ethylene glycol dimethyl ether; water T=80°C;
参考文献
Diaz, Caroline Jean; Haffner, Curt Dale; Speake, Jason Daniel; Zhang, Cunyu; Mills, Wendy Yoon; Spearing, Paul Kenneth; Cowan, David John; Green, Gary Martin
Patent: US2010/222345 A1, 2010 ;
Location in patent: Page/Page column 83 ;
反应条件
potassium phosphate; oxygen; palladium diacetate; copper(ll) bromide; 2,2,2-trimethylacetic acid in N,N-dimethyl acetamide
T=120°C; P=760.051 Torr; 24 h;
参考文献
Wu, Ge; Zhou, Jun; Zhang, Min; Hu, Peng; Su, Weiping
Chemical Communications, 2012 , vol. 48, # 71 p. 8964 - 8966
反应条件
1: C27H37ClCuN3; potassium tert-butylate / tetrahydrofuran / 8 h / 80 °C / 760.05 Torr / Inert atmosphere; sealed tube
2: N,N-dimethyl-formamide / 1 h / 80 °C / Inert atmosphere; sealed tube
View Scheme
参考文献
Inomata, Hiroshi; Ogata, Kenichi; Fukuzawa, Shin-Ichi; Hou, Zhaomin
Organic Letters, 2012 , vol. 14, # 15 p. 3986 - 3989
反应条件
C27H37ClCuN3; potassium tert-butylate in tetrahydrofuran
T=80°C; P=760.051 Torr; 8 h; Inert atmospheresealed tube;
参考文献
Inomata, Hiroshi; Ogata, Kenichi; Fukuzawa, Shin-Ichi; Hou, Zhaomin
Organic Letters, 2012 , vol. 14, # 15 p. 3986 - 3989
