反应条件
1.1: silver carbonate; 1,10-phenanthroline; copper(l) chloride; potassium tert-butylate / N,N-dimethyl-formamide / 1 h / 40 °C / |Inert atmosphere; |Glovebox 1.2: 40 °C / |Inert atmosphere; |Glovebox 1.3: 20 °C / |Inert atmosphere 2.1: toluene / 24 h / 70 °C / |Inert atmosphere 3.1: water; 1,8-diazabicyclo[5.4.0]undec-7-ene / nitromethane / 2 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Aiguabella, Nuria; Del Pozo, Carlos; Verdaguer, Xavier; Fustero, Santos; Riera, Antoni
Angewandte Chemie - International Edition, 2013 , vol. 52, # 20 p. 5355 - 5359
Angew. Chem., 2013 , vol. 125, # 20 p. 5463 - 5467,5
