1: NaH / dimethylformamide / 6 h / 0 °C 2: HCl(g) / CH2Cl2 / 0.17 h / 0 - 5 °C 3: TMSBr / CH2Cl2 / 18 h / Ambient temperature 4: conc. NH4OH / 4 h / Ambient temperature View Scheme
参考文献
Brodfuehrer, Paul R.; Howell, Henry G.; Sapino, Chester Jr.; Vemishetti, Purushotham
Tetrahedron Letters, 1994 , vol. 35, # 20 p. 3243 - 3246
