1-(2-氟苯基)1H-吡咯-2-甲醛合成路线 (共 4 条)
反应条件
trichlorophosphate T=50°C; Vilsmeier-Haak formylation; 3 h;
参考文献
Sanchez, Isabel; Pujol, Maria Dolors
Tetrahedron, 1999 , vol. 55, # 17 p. 5593 - 5598
反应条件
1: glacial acetic acid / 1 h / 115 °C 2: oxalyl chloride / 1,2-dichloro-ethane / 0.5 h / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 21, # 15-16 p. 1567 - 1576
反应条件
oxalyl dichloride in 1,2-dichloro-ethane 0.5 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Synthetic Communications, , vol. 21, # 15-16 p. 1567 - 1576
反应条件
sodium tetrahydroborate in methanol T=20°C; Reduction; 0.5 h;
参考文献
Sanchez, Isabel; Pujol, Maria Dolors
Tetrahedron, 1999 , vol. 55, # 17 p. 5593 - 5598