2,2,6,6-四甲基-1-(1-苯基乙氧基)合成路线 (共 9 条)
反应条件
dihydrogen peroxide; copper(l) chloride in tert-butyl alcohol T=20°C; 13 h;
参考文献
Schoening, Kai-Uwe; Fischer, Walter; Hauck, Stefan; Dichtl, Alexander; Kuepfert, Michael
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1567 - 1573
反应条件
1: 4-hydroxy-2,2,6,6-tetramethyl piperidinyloxy, free radical With N,N,N',N'',N''-pentamethyldiethylenetriamine; copper; copper(I) bromide in methoxybenzene 0.0833333 h; 2: 1-bromo-1-phenyl-ethane in methoxybenzene 18 h;
参考文献
Nicolay, Renaud; Matyjaszewski, Krzysztof
Macromolecules, 2011 , vol. 44, # 2 p. 240 - 247
反应条件
1: 41 percent / di-tert-butylperoxide / 16 h / Heating 2: 81 percent / aq. KOH / ethanol / 16 h / Heating View Scheme
参考文献
Hawker, Craig J.; Barclay, George G.; Dao, Julian
Journal of the American Chemical Society, 1996 , vol. 118, # 46 p. 11467 - 11471
反应条件
1: 41 percent / di-tert-butylperoxide / 16 h / Heating 2: 81 percent / aq. KOH / ethanol / 16 h / Heating View Scheme
参考文献
Hawker, Craig J.; Barclay, George G.; Dao, Julian
Journal of the American Chemical Society, 1996 , vol. 118, # 46 p. 11467 - 11471
参考文献
Babiarz, Joseph E.; Cunkle, Glen T.; DeBellis, Anthony D.; Eveland, David; Pastor, Stephen D.; Shum, Sai P.
Journal of Organic Chemistry, 2002 , vol. 67, # 19 p. 6831 - 6834
反应条件
in acetonitrile T=140°C; Kinetics;
参考文献
Goto, Atsushi; Kwak, Yungwan; Yoshikawa, Chiaki; Tsujii, Yoshinobu; Sugiura, Yukio; Fukuda, Takeshi
Macromolecules, 2002 , vol. 35, # 9 p. 3520 - 3525
反应条件
oxygen in various solvent(s) T=133.85°C; Kinetics;
参考文献
Schulte, Tobias; Studer, Armido
Macromolecules, 2003 , vol. 36, # 9 p. 3078 - 3084
反应条件
in acetonitrile T=110 - 125°C; Kinetics;
参考文献
Fischer, Hanns; Kramer, Andreas; Marque, Sylvain R. A.; Nesvadba, Peter
Macromolecules, 2005 , vol. 38, # 24 p. 9974 - 9984
反应条件
in acetonitrile
T=110 - 125°C; Kinetics;
参考文献
Fischer, Hanns; Kramer, Andreas; Marque, Sylvain R. A.; Nesvadba, Peter
Macromolecules, 2005 , vol. 38, # 24 p. 9974 - 9984