反应条件
1: 85 percent / m-ClC6H4CO3H / CH2Cl2 / 3 h / 0 °C 2: 84 percent / LiAlD4 / tetrahydrofuran / 6 h / 0 - 20 °C 3: 78 percent / Jones reagent / acetone / 0.25 h / 0 °C 4: SOCl2, collidine / tetrahydrofuran / 0.17 h / 0 °C 5: 1.) DIBAL-H; 2.) Me2CO, iPrOH / 1.) 0 deg C; 2.) 20 deg C View Scheme
参考文献
Holland, Herbert L.; Rao, J. Appa; Chenchaiah, P. Chinna
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2027 - 2032
