1: caesium carbonate / N,N-dimethyl-formamide / 30 h / 30 °C / Inert atmosphere 2: lithium aluminium tetrahydride / tetrahydrofuran / 72 h / Inert atmosphere; Reflux View Scheme

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '8127930', constants.ctx, '0')">sodium iodide</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '635680', constants.ctx, '0')">acetone</a> <br />3&nbsp;h;&nbsp;&nbsp;Inert atmosphereReflux;&nbsp;<br /> &nbsp;