反应条件
1: 6,7-dimethoxy-3,4-dihydro-1H-isochromene With 2,3-dicyano-5,6-dichloro-p-benzoquinone; bis-[(trifluoroacetoxy)iodo]benzene in 1,2-dichloro-ethane T=80°C; 3 h; Inert atmosphere; 2: PhMgI in diethyl ether; 1,2-dichloro-ethane T=-20°C; 3 h; Inert atmosphere;
参考文献
Muramatsu, Wataru; Nakano, Kimihiro
Organic Letters, 2014 , vol. 16, # 7 p. 2042 - 2045