反应条件
in n-heptane byproducts: NaCl; reagents mixed in heptane at -78°C, after 6 h, react. mixt. warmed to room temp.; volatiles removed, filtered, volume reduced, within 1 day at -23°C crystals obtained;
参考文献
Wiberg, Nils; Blank, Thomas; Amelunxen, Kerstin; Noeth, Heinrich; Knizek, Joerg; Habereder, Tassilo; Kaim, Wolfgang; Wanner, Matthias
European Journal of Inorganic Chemistry, 2001 , # 7 p. 1719 - 1727
