1,1,1,3-四氯丁烷合成路线 （共 26 条）
反应条件
triethylsilane; pentacarbonyliron(0)
参考文献
Vasil'eva,T.T. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1979 , vol. 28, p. 1428 - 1431
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1979 , vol. 28, p. 1543 - 1548
反应条件
sodium hydroxide; tetrabutylammomium bromide in water T=20°C; 24 h;
参考文献
HIF BIO, INC.; BIZBIOTECH CO., LTD.
Patent: WO2007/65010 A2, 2007 ;
Location in patent: Page/Page column 118 ;
WO 2007/065010 A2
反应条件
sodium hydroxide; tetrabutylammomium bromide in water
参考文献
Bayer Aktiengesellschaft
Patent: US6166027 A1, 2000 ;
反应条件
2,2'-azo-bisisobutyronitrile
参考文献
Ziegler
Patent: DE864866 , 1950 ;
Full Text Show Details
Sladkow et al.
Khimicheskaya Nauka i Promyshlennost, 1957 , vol. 2, p. 669
Chem.Abstr., 1958 , p. 6148
反应条件
carbon monoxide; [Fe(cyclopentadienyl(CO)2)]2
T=53°C; P=147102 Torr;
参考文献
Susuki,T.; Tsuji,J.
Tetrahedron Letters, 1968 , p. 913 - 915
反应条件
potassium carbonate; palladium diacetate; triphenylphosphine
P=30400 Torr; 96 h; Ambient temperature;
参考文献
Tsuji, Jiro; Sato, Koji; Nagashima, Hideo
Tetrahedron, 1985 , vol. 41, # 21 p. 5003 - 5006
反应条件
[Fe(cyclopentadienyl(CO)2)]2
T=53°C; P=147102 Torr;
参考文献
Susuki,T.; Tsuji,J.
Tetrahedron Letters, 1968 , p. 913 - 915
反应条件
anhydrous diethylamine hydrochloride; 1,2-diphenyl-2-hydroxyethanone; iron(III) chloride in isopropyl alcohol
Further byproducts given;
参考文献
Moore,L.O.
Journal of Organic Chemistry, 1972 , vol. 37, p. 2633 - 2635
反应条件
1,2-diphenyl-2-hydroxyethanone; diethylamine; iron(III) chloride in isopropyl alcohol
Further byproducts given;
参考文献
Moore,L.O.
Journal of Organic Chemistry, 1972 , vol. 37, p. 2633 - 2635
反应条件
chlorine in carbon disulfide
T=25°C; Irradiation;
参考文献
Burton,T.; Bruylants,A.
Bulletin des Societes Chimiques Belges, 1972 , vol. 81, p. 639 - 642
