2-环己基-2-氧代乙酸乙酯合成路线 (共 16 条)
反应条件
magnesium in tetrahydrofuran T=-78°C; Grignard reaction; 0.5 h;
参考文献
Rochat, Sabine; Minardi, Caroline; De Saint Laumer, Jean-Yves; Herrmann, Andreas
Helvetica Chimica Acta, 2000 , vol. 83, # 7 p. 1645 - 1671
参考文献
Senanayake, Chris H.; Fang, Kevin; Grover, Paul; Bakale, Roger P.; Vandenbossche, Charles P.; Wald, Stephen A.
Tetrahedron Letters, 1999 , vol. 40, # 5 p. 819 - 822
反应条件
zinc(II) chloride in diethyl ether 23 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 1231 - 1232
反应条件
in tetrahydrofuran; diethyl ether T=-80 - -60°C; 1 h;
参考文献
Boivin, Stephane; Outurquin, Francis; Paulmier, Claude
Tetrahedron, 1997 , vol. 53, # 49 p. 16767 - 16782
反应条件
in diethyl ether T=-90°C; 1 h;
参考文献
Heterocycles, , vol. 49, # 1 p. 459 - 464
反应条件
in diethyl ether T=-78°C; Inert atmosphere;
参考文献
Hayashi, Masashi; Nakamura, Shuichi
Angewandte Chemie - International Edition, 2011 , vol. 50, # 10 p. 2249 - 2252
反应条件
potassium tert-butylate; oxygen in N,N-dimethyl-formamide
参考文献
Journal of Organic Chemistry, , vol. 35, # 10 p. 3240 - 3243
反应条件
1: NaBH4 2: KOtBu, O2 / dimethylformamide View Scheme
参考文献
Journal of Organic Chemistry, , vol. 35, # 10 p. 3240 - 3243
反应条件
1: N-chlorosuccinimide / CCl4 / 2 h / Heating 2: 66 percent / Hg(OAc)2 / acetone; H2O / 1 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 56, # 38 p. 7495 - 7502
反应条件
sulfuric acid in benzene
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 29, p. 97 - 120