4,5-双(2-氰乙基硫代)-1,3-二硫醇-2-硫酮合成路线 （共 11 条）
反应条件
pyridine hydrochloride in acetonitrile T=50 - 60°C; 2 h;
参考文献
Jia, Chunyang; Zhang, Deqing; Xu, Wei; Zhu, Daoben
Organic Letters, 2001 , vol. 3, # 12 p. 1941 - 1943
反应条件
in acetonitrile 1 h; Heating;
参考文献
Pacsial, Eden J.; Alexander, Daniel; Alvarado, Robert J.; Tomasulo, Massimiliano; Raymo, Francisco M.
Journal of Physical Chemistry B, 2004 , vol. 108, # 50 p. 19307 - 19313
反应条件
pyridine hydrochloride in acetonitrile T=50 - 60°C; 2 h;
参考文献
Jia, Chunyang; Zhang, Deqing; Guo, Xuefeng; Wan, Shuhui; Xu, Wei; Zhu, Daoben
Synthesis, 2002 , # 15 p. 2177 - 2182
参考文献
Tatewaki, Yoko; Watanabe, Takanori; Watanabe, Koji; Kikuchi, Kohei; Okada, Shuji
Dalton Transactions, 2013 , vol. 42, # 45 p. 16121 - 16127
反应条件
in acetone 2 h; Heating;
参考文献
Abashev, G. G.; Russkikh, V. S.; Shklyaeva, E. V.; Vladykin, V. I.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 11 p. 1533 - 1537
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 11 p. 1705 - 1710
反应条件
1: 48 percent / mercury acetate / acetic acid 2: triethylphosphite / 1 h / Heating View Scheme
参考文献
Abashev, G. G.; Russkikh, V. S.; Shklyaeva, E. V.; Vladykin, V. I.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 11 p. 1533 - 1537
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 11 p. 1705 - 1710
反应条件
mercury(II) diacetate in chloroform; acetic acid
参考文献
Xu, Ming; Ji, Yong; Zuo, Jing-Lin; Li, Yi-Zhi; You, Xiao-Zeng
Journal of Heterocyclic Chemistry, 2005 , vol. 42, # 5 p. 847 - 850
反应条件
in chloroform; acetic acid
参考文献
Tatewaki, Yoko; Watanabe, Takanori; Watanabe, Koji; Kikuchi, Kohei; Okada, Shuji
Dalton Transactions, 2013 , vol. 42, # 45 p. 16121 - 16127
反应条件
triethyl phosphite
T=135°C; Substitution; 1 h;
参考文献
Jeppesen, Jan Oskar; Takimiya, Kazuo; Jensen, Frank; Brimert, Thomas; Nielsen, Kent; Thorup, Niels; Becher, Jan
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5794 - 5805
反应条件
1: 48 percent / mercury acetate / acetic acid
2: 68 percent / triethyl phosphite / 2 h / Heating
View Scheme
参考文献
Svenstrup; Rasmussen; Hansen; Becher
Synthesis, 1994 , # 8 p. 809 - 812
