2,3,6,7-四(2-氰乙基硫代)四硫富瓦烯合成路线 （共 13 条）
反应条件
sodium 1.) EtOH, r.t., 4 h; 2.) EtOH, r.t., 45 min; Yield given. Multistep reaction;
参考文献
Synthesis, , # 8 p. 809 - 812
反应条件
sodium 1.) EtOH, r.t., 4 h; 2.) EtOH, r.t., overnight; Yield given. Multistep reaction;
参考文献
Svenstrup; Rasmussen; Hansen; Becher
Synthesis, 1994 , # 8 p. 809 - 812
反应条件
triethyl phosphite in toluene
T=90°C; 3 h; Inert atmosphere;
参考文献
Rabaca, Sandra; Oliveira, Sandrina; Santos, Isabel C.; Almeida, Manuel
Tetrahedron Letters, 2013 , vol. 54, # 48 p. 6635 - 6639
反应条件
triethyl phosphite in toluene
0.5 h; Heating;
参考文献
Binet, Laurent; Fahre, Jean Marc; Montginoul, Claude; Simonsen, Klaus Baek; Becher, Jan
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 8 p. 783 - 788
反应条件
triethyl phosphite
T=135°C; Substitution; 1 h;
参考文献
Jeppesen, Jan Oskar; Takimiya, Kazuo; Jensen, Frank; Brimert, Thomas; Nielsen, Kent; Thorup, Niels; Becher, Jan
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5794 - 5805
反应条件
triethyl phosphite
T=120°C; 2 h; Inert atmosphere;
参考文献
Skibinski, Maciej; Gomez, Rafael; Lork, Enno; Azov, Vladimir A.
Tetrahedron, 2009 , vol. 65, # 50 p. 10348 - 10354
反应条件
1: 48 percent / mercury acetate / acetic acid
2: 68 percent / triethyl phosphite / 2 h / Heating
View Scheme
参考文献
Abashev, G. G.; Russkikh, V. S.; Shklyaeva, E. V.; Vladykin, V. I.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 11 p. 1533 - 1537
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 11 p. 1705 - 1710
反应条件
triethyl phosphite
T=100°C; 1.5 h;
参考文献
Binet, Laurent; Fahre, Jean Marc; Montginoul, Claude; Simonsen, Klaus Baek; Becher, Jan
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 8 p. 783 - 788
反应条件
triethyl phosphite
T=100°C; 1.5 h; Yields of byproduct given;
参考文献
Binet, Laurent; Fahre, Jean Marc; Montginoul, Claude; Simonsen, Klaus Baek; Becher, Jan
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 8 p. 783 - 788
反应条件
triethyl phosphite
Heating;
参考文献
Abashev; Bushueva; Lebedev; Shklyaeva
Russian Journal of Organic Chemistry, 2007 , vol. 43, # 1 p. 135 - 147
