3,4-二氢-6,7-二甲氧基-4-甲基-3-氧代-2-喹喔啉丙酸合成路线 (共 2 条)
反应条件
Yield given. Multistep reaction;
参考文献
Shimizu, Masato; Takahashi, Tomohiko; Uratsuka, Satoru; Yamada, Sachiko
Journal of the Chemical Society, Chemical Communications, 1990 , # 20 p. 1416 - 1417
反应条件
1: diphenylphosphoryl azide (DPPA), Et3N / dimethylformamide 2: benzene / 1 h / Heating 3: benzene / 0.5 h / Heating 4: 81 percent / K2CO3 / ethanol / 6 h / Heating 5: 100 percent / PhI(OAc)2 / CH2Cl2 / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 20 p. 1416 - 1417