4,4,4-三氯-1-丁烯合成路线 （共 18 条）
反应条件
ethanolamine; copper(l) chloride in tert-butyl alcohol
T=80°C; Alkylation; 50 h;
参考文献
Mitani, Michiharu; Hujita, Shigenori
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 12 p. 3055 - 3060
参考文献
Sakurai,H. et al.
Journal of Organic Chemistry, 1969 , vol. 34, p. 1764 - 1768
反应条件
PPh3-Pd-C6HCl4; 1,2-bis-(diphenylphosphino)ethane in dichloromethane
5 h; Ambient temperature;
参考文献
Kurosawa, Hideo; Urabe, Akira
Chemistry Letters, 1985 , p. 1839 - 1840
反应条件
azobisisobutyronitrile in benzene
T=100°C; 1 h; other temperatures, other catalysts;
参考文献
Kosugi, Masanori; Kurata, Hiroshi; Kawata, Ken-ichi; Migita, Toshihiko
Chemistry Letters, 1991 , # 8 p. 1327 - 1328
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride
T=40°C; 5 h; Further byproducts given;
参考文献
Mandel'shtam, T. V.; Kharicheva, E. M.; Labeish, N. N.; Kostikov, R. R.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 2143 - 2148
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 12 p. 2513 - 2518
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride
T=40°C; 5 h; Further byproducts given;
参考文献
Mandel'shtam, T. V.; Kharicheva, E. M.; Labeish, N. N.; Kostikov, R. R.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 2143 - 2148
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 12 p. 2513 - 2518
反应条件
T=30 - 40°C; im Quecksilbedampf-Neonlicht;
参考文献
Kharasch; Sage
Journal of Organic Chemistry, 1949 , vol. 14, p. 80,82
反应条件
azobisisobutyronitrile in benzene
T=80°C; 3 h; other negatively substituted aliphatic halides, var. tin compounds, reagents, solvents, temp. and time, also with irradiation; Product distribution;
参考文献
Migita; Nagai; Kosugi
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2480 - 2484
反应条件
trichloromonobromomethane; dibenzoyl peroxide
参考文献
Sakurai,H. et al.
Journal of Organic Chemistry, 1969 , vol. 34, p. 1764 - 1768
反应条件
in benzene-d6
6 h; Irradiation;
参考文献
Russell, Glen A.; Herold, Lourdes Lucas
Journal of Organic Chemistry, 1985 , vol. 50, # 7 p. 1037 - 1040
