N-(二苯基亚甲基)-甲胺合成路线 (共 40 条)
反应条件
1: bei aufeinanderfolgender Umsetzung mit CH3I und mit Benzylmagnesiumchlorid 2: toluene-4-sulfonic acid methyl ester; ethanol View Scheme
参考文献
Hauser et al.
Journal of Organic Chemistry, 1955 , vol. 20, p. 1119,1125
反应条件
(i) LDA, THF, heptane, (ii) /BRN= 1730892/; Multistep reaction;
参考文献
Popowski,E. et al.
Journal of Organometallic Chemistry, 1976 , vol. 110, p. 295 - 302
反应条件
in benzene T=50 - 55°C; 1 h;
参考文献
Ivanova, Ginka G.
Tetrahedron, 1992 , vol. 48, # 1 p. 177 - 186
反应条件
in benzene T=50 - 55°C; 1 h; variation of mol. ratio, time; Product distributionMechanism;
参考文献
Ivanova, Ginka G.
Tetrahedron, 1992 , vol. 48, # 1 p. 177 - 186
反应条件
(i) LiNEt2, HMPT, benzene, (ii) /BRN= 1098373/, (iii) aq. HCl; Multistep reaction;
参考文献
Hullot,P.; Cuvigny,T.
Bulletin de la Societe Chimique de France, 1973 , p. 2989 - 2992
反应条件
sodium tetrahydroborate in isopropyl alcohol T=60 - 70°C; 3 h;
参考文献
Quast, Helmut; Hergenroether, Thomas
Chemische Berichte, 1992 , vol. 125, # 11 p. 2625 - 2628
反应条件
(i) LiNEt2, HMPT, benzene, (ii) /BRN= 507487/, (iii) aq. HCl; Multistep reaction;
参考文献
Hullot,P.; Cuvigny,T.
Bulletin de la Societe Chimique de France, 1973 , p. 2989 - 2992
反应条件
in benzene
T=50 - 55°C; 1 h;
参考文献
Ivanova, Ginka G.
Tetrahedron, 1992 , vol. 48, # 1 p. 177 - 186
反应条件
oxaziridinium tetrafluoroborate derived from N-methyl-1,2,3,4-tetrahydroisoquinoline in dichloromethane
1.5 h; Ambient temperature;
参考文献
Hanquet, Gilles; Lusinchi, Xavier
Tetrahedron, 1994 , vol. 50, # 42 p. 12185 - 12200
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=0°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Boyd, Derek R.; Coulter, Peter B.; McGuckin, M. Rosaleen; Sharma, Narain D.; Jennings, W. Brian; Wilson, Valerie E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 2 p. 301 - 306