1,2,3-三-O-苯甲酰基-4,6-二脱氧吡喃己糖合成路线 (共 2 条)
反应条件
Multi-step reaction with 3 steps 1: 65 percent / pyridine / 0.2 h / -40 °C2: sodium iodide / dimethylformamide / Ambient temperature3: 85 percent / triethylamine, H2 / 10percent Pd-C / methanol; CH2Cl2 / 30 h / Ambient temperature
参考文献
Lindhorst, Thisbe K.; Thiem, Joachim Carbohydrate Research, 1991 , vol. 209, p. 119 - 129
反应条件
Multi-step reaction with 3 steps 1: 65 percent / pyridine / 0.2 h / -40 °C2: sodium iodide / dimethylformamide / Ambient temperature3: 85 percent / triethylamine, H2 / 10percent Pd-C / methanol; CH2Cl2 / 30 h / Ambient temperature
参考文献
Lindhorst, Thisbe K.; Thiem, Joachim Carbohydrate Research, 1991 , vol. 209, p. 119 - 129