4-硝基苯基-2-羟基乙基硫化物合成路线 （共 17 条）
反应条件
1: 86 percent / hydrogen peroxide (30percent) / Na2WO4*2H2O / ethanol; H2O / 1 h / Heating 2: 99 percent / tetrahydrofuran / -78 - 20 °C View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 107, p. 621 - 626
反应条件
phosphorus pentachloride
参考文献
Bennett; Berry
Journal of the Chemical Society, 1927 , p. 1680
参考文献
Flowers,W.T. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1979 , p. 1309 - 1321
反应条件
1: MnSO4; aq. H2O2; NaHCO3 / acetonitrile / 20 °C
2: 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; DMAP / CH2Cl2 / 12 h / 20 °C
3: aq. NaHCO3 / acetone / 12 h / 20 °C
View Scheme
参考文献
Claesen, C. A. A.; Pistorius, A. M. A.; Tesser, G. I.
Tetrahedron Letters, 1985 , vol. 26, # 32 p. 3859 - 3862
反应条件
phosphorus pentachloride
参考文献
Bennett; Berry
Journal of the Chemical Society, 1927 , p. 1680
反应条件
hydrogenchloride; sodium hypochlorite
参考文献
McDowell,S.T.; Stirling,C.J.M.
Journal of the Chemical Society [Section] B: Physical Organic, 1967 , p. 348 - 350
反应条件
1: MCPBA / CH2Cl2 / 2 h / 0 °C
2: SnCl2*2H2O / ethanol / 12 h / Heating
View Scheme
参考文献
Chou, Shang-Shing P.; Yu, Chiung-Yi; Lin, Hong-Cheu; Yang, Pao-Keng
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 3 p. 487 - 492
