5-三氟甲基苯并[b]噻吩合成路线 (共 4 条)
反应条件
hydrogen sulfide; acetylene T=670°C; 0.0180556 h; Yield given. Yields of byproduct given;
参考文献
Russian Journal of Organic Chemistry, , vol. 29, # 11.2 p. 1863 - 1867
Zhurnal Organicheskoi Khimii, , vol. 29, # 11 p. 2246 - 2250
反应条件
hydrogen sulfide T=670°C; 0.0180556 h; Yield given. Yields of byproduct given;
参考文献
Russian Journal of Organic Chemistry, , vol. 29, # 11.2 p. 1863 - 1867
Zhurnal Organicheskoi Khimii, , vol. 29, # 11 p. 2246 - 2250
反应条件
T=630°C; 0.0175 h; gas phase copyrolysis; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, p. 1516 - 1522
Zhurnal Organicheskoi Khimii, , vol. 18, # 8 p. 1736 - 1743
反应条件
4,4'-di-tert-butyl-2,2'-dipyridyl; bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I) in hexane T=20°C; 4 h; Inert atmosphere;
参考文献
JANSSEN PHARMACEUTICA N.V.
Patent: WO2009/105220 A1, 2009 ;
Location in patent: Page/Page column 43-44 ;
WO 2009/105220 A1