(S)-3-[(甲基磺酰基)氧基]吡咯烷-1-羧酸叔丁酯合成路线 （共 16 条）
反应条件
1: With sodium hydride in N,N-dimethyl-formamide T=60°C; 2: With hydrogenchloride Further stages. Title compound not separated from byproducts.;
参考文献
Benard, Christophe; Mohammad, Rahim; Saraswat, Neerja; Shan, Rudong; Maiti, Samarendra N.; Wuts, Peter G. M.; Stier, Michael; Lints, Teresa; Bradow, James; Schwarz, Jacob B.
Synthetic Communications, 2008 , vol. 38, # 4 p. 517 - 524
反应条件
1: With sodium hydride in N,N-dimethyl-formamide T=60°C; 2: With hydrogenchloride in 1,4-dioxane T=20°C; 0.5 h; Further stages. Title compound not separated from byproducts.;
参考文献
Benard, Christophe; Mohammad, Rahim; Saraswat, Neerja; Shan, Rudong; Maiti, Samarendra N.; Wuts, Peter G. M.; Stier, Michael; Lints, Teresa; Bradow, James; Schwarz, Jacob B.
Synthetic Communications, 2008 , vol. 38, # 4 p. 517 - 524
反应条件
sodium hydride in N,N-dimethyl-formamide T=60°C; Title compound not separated from byproducts.;
参考文献
Benard, Christophe; Mohammad, Rahim; Saraswat, Neerja; Shan, Rudong; Maiti, Samarendra N.; Wuts, Peter G. M.; Stier, Michael; Lints, Teresa; Bradow, James; Schwarz, Jacob B.
Synthetic Communications, 2008 , vol. 38, # 4 p. 517 - 524
反应条件
sodium hydride in N,N-dimethyl-formamide T=60°C; Title compound not separated from byproducts.;
参考文献
Benard, Christophe; Mohammad, Rahim; Saraswat, Neerja; Shan, Rudong; Maiti, Samarendra N.; Wuts, Peter G. M.; Stier, Michael; Lints, Teresa; Bradow, James; Schwarz, Jacob B.
Synthetic Communications, 2008 , vol. 38, # 4 p. 517 - 524
反应条件
1: dimethylformamide 2: NH3 / methanol 3: pyridine / CH2Cl2 View Scheme
参考文献
Kocalka, Petr; Pohl, Radek; Rejman, Dominik; Rosenberg, Ivan
Tetrahedron, 2006 , vol. 62, # 24 p. 5763 - 5774
反应条件
in N,N-dimethyl-formamide T=110°C; 72 h;
参考文献
Kocalka, Petr; Pohl, Radek; Rejman, Dominik; Rosenberg, Ivan
Nucleosides, Nucleotides and Nucleic Acids, 2005 , vol. 24, # 5-7 p. 805 - 808
反应条件
1: in water; toluene T=80°C; P=1500.15 Torr; 18 h; 2: With hydrogenchloride in water; isopropyl alcohol
参考文献
Kaneka Corporation
Patent: EP2050735 A1, 2009 ;
Location in patent: Page/Page column 20 ;
反应条件
1: dimethylformamide 2: NH3 / methanol View Scheme
参考文献
Kocalka, Petr; Pohl, Radek; Rejman, Dominik; Rosenberg, Ivan
Tetrahedron, 2006 , vol. 62, # 24 p. 5763 - 5774
反应条件
1: dimethylformamide 2: NH3 / methanol View Scheme
参考文献
Kocalka, Petr; Pohl, Radek; Rejman, Dominik; Rosenberg, Ivan
Tetrahedron, 2006 , vol. 62, # 24 p. 5763 - 5774
反应条件
ammonia in water T=80 - 90°C; P=3000.3 - 6000.6 Torr; 10 - 19 h; Product distribution / selectivity;
参考文献
Kaneka Corporation
Patent: EP2050735 A1, 2009 ;
Location in patent: Page/Page column 19-20 ;
