3-甲基-2-喹喔啉羧酸乙酯 1,4-二氧化物合成路线 （共 18 条）
反应条件
selenium(IV) oxide in ethyl acetate
4 h; Heating;
参考文献
Monge Vega; Gil; Fernandez-Alvarez
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 5 p. 1271 - 1276
反应条件
reduction of Dirlam and McFarland;
参考文献
Gomes, Jose R. B.; Monteiro, Andre R.; Campos, Bruno B.; Gomes, Paula; Ribeiro Da Silva, Maria D. M. C.
Journal of Physical Organic Chemistry, 2009 , vol. 22, # 1 p. 17 - 23
反应条件
sodium dithionite in methanol; water
T=40°C; 6 h;
参考文献
Stumm, Gerhard; Niclas, Hans-Joachim
Zeitschrift fuer Chemie (Stuttgart, Germany), 1989 , vol. 29, # 6 p. 208 - 209
反应条件
1: Cl2 / acetic acid / 80 - 85 °C
2: 90 percent hydrazine hydrate / ethanol; H2O / 24 h / Ambient temperature
3: phosphorus pentasulfide / pyridine / 6 h / Heating
4: hydrazine / ethanol / 4 h / Heating
View Scheme
参考文献
Monge Vega; Gil; Fernandez-Alvarez
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 5 p. 1271 - 1276
反应条件
1: trimethylphosphite / propan-1-ol / 1.5 h / Heating
2: aq. NaOH / 3 h / Heating
View Scheme
参考文献
Li, Jian-Yong; Zhang, Ji-Yu; Zhou, Xu-Zheng; Li, Jin-Shan; Lu, Run-Hua
Heterocyclic Communications, 2007 , vol. 13, # 1 p. 49 - 56
反应条件
hydrazine hydrate in ethanol
3 h; Reflux;
参考文献
Romeiro, Nelilma C.; Aguirre, Gabriela; Hernandez, Paola; Gonzalez, Mercedes; Cerecetto, Hugo; Aldana, Ignacio; Perez-Silanes, Silvia; Monge, Antonio; Barreiro, Eliezer J.; Lima, Lidia M.
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 2 p. 641 - 652
反应条件
1: Cl2 / acetic acid / 80 - 85 °C
2: 90 percent hydrazine hydrate / ethanol; H2O / 24 h / Ambient temperature
View Scheme
参考文献
Monge Vega; Gil; Fernandez-Alvarez
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 5 p. 1271 - 1276
反应条件
triethylamine; calcium chloride in methanol
T=50°C; 2 h;
参考文献
Stumm, G.; Niclas, H.-J.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 5 p. 736 - 744
