1: 1) NaH, 2) LiAlH4 / 1) DME, refl., 4 h, 2) r.t., 12 h
2: 67 percent / (+)-diethyl tartrate, titanium isopropoxide, tBuOOH / CH2Cl2 / 24 h / -20 °C
3: 94 percent / LiAlH4 / diethyl ether / 12 h / Ambient temperature
View Scheme
参考文献
Yadav, J. S.; Satyanarayana Reddy, P.; Jolly, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 294 - 295
