2-(2-甲氧基苯基)-1,3-二恶烷合成路线 （共 5 条）
反应条件
ruthenium trichloride; sodium sulfate T=20°C; 10 h;
参考文献
Tetrahedron Letters, , vol. 45, # 41 p. 7719 - 7721
反应条件
diisobutylaluminium hydride in toluene T=0 - 20°C; 18 h;
参考文献
WARNER-LAMBERT COMPANY LLC
Patent: WO2004/89915 A1, 2004 ;
Location in patent: Page 65; 67 ;
反应条件
lithium trifluoromethane sulfonate T=90°C; 4 h;
参考文献
Firouzabadi, Habib; Eslami, Shahram; Karimi, Babak
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 12 p. 2401 - 2406
反应条件
1: 98 percent / diisobutylaluminium hydride / toluene / 18 h / 0 - 20 °C
2: 27 percent / dimethylaminopyridine; pyridine / CH2Cl2 / 24 h / Heating
View Scheme
参考文献
Cody, Wayne L.; Holsworth, Daniel D.; Powell, Noel A.; Jalaie, Mehran; Zhang, Erli; Wang, Wei; Samas, Brian; Bryant, John; Ostroski, Robert; Ryan, Michael J.; Edmunds, Jeremy J.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 1 p. 59 - 68
反应条件
1: 98 percent / diisobutylaluminium hydride / toluene / 18 h / 0 - 20 °C
2: 27 percent / dimethylaminopyridine; pyridine / CH2Cl2 / 24 h / Heating
3: 100 percent / lithium iodide / acetone / 1 h / Heating
View Scheme
参考文献
Cody, Wayne L.; Holsworth, Daniel D.; Powell, Noel A.; Jalaie, Mehran; Zhang, Erli; Wang, Wei; Samas, Brian; Bryant, John; Ostroski, Robert; Ryan, Michael J.; Edmunds, Jeremy J.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 1 p. 59 - 68
