反应条件
magnesium in tetrahydrofuran byproducts: MgClBr; Sonication; the mixt. of magnesium, germane and halogen-compound in THF was sonicated for 2 h (inert atm.); the mixt. was washed with satd. soln. of NaCl, extd. with diethyl ether,the organic layer was dried over MgSO4, the solvent was removed under r educed pressure, column chromy. (petroleum ether-diethyl ether 95/5);
参考文献
Langle, Sandrine; David-Quillot, Franck; Balland, Alexia; Abarbri, Mohamed; Duchene, Alain
Journal of Organometallic Chemistry, 2003 , vol. 671, # 1-2 p. 113 - 119
