2-溴-3,5-二甲氧基甲苯合成路线 (共 16 条)
反应条件
N-bromosuccinmide in tetrachloromethane 4 h; Heating;
参考文献
Mondal, Mukulesh; Puranik, Vedavati G.; Argade, Narshinha P.
Journal of Organic Chemistry, 2007 , vol. 72, # 6 p. 2068 - 2076
反应条件
potassium carbonate in acetone T=20°C; 24 h;
参考文献
Hamad Elgazwy, Abdel-Sattar S.
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 164, p. 131 - 143
反应条件
1: 82 percent / potassium carbonate / acetone / 7 h / Heating 2: 68 percent / copper(II) bromide / 1,2-dimethoxy-ethane / 2 h View Scheme
参考文献
Insole, Joan M.
Journal of Chemical Research, Miniprint, 1990 , # 12 p. 2831 - 2867
参考文献
Calam; Oxford
Journal of the Chemical Society, 1939 , p. 280,283
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Asahina; Fuzikawa
Chemische Berichte, 1934 , vol. 67, p. 163,166, 715
Yakugaku Zasshi, 1934 , vol. 54, p. 223,228
反应条件
1: CCl4; bromine; N-bromo-succinimide / Irradiation 2: quinoline; copper-powder View Scheme
参考文献
Logan; Newbold
Journal of the Chemical Society, 1957 , p. 1946,1949
反应条件
sodium hydroxide auf dem Dampfbad;
参考文献
Asahina; Fuzikawa
Chemische Berichte, 1934 , vol. 67, p. 163,166, 715
Yakugaku Zasshi, 1934 , vol. 54, p. 223,228
反应条件
L-proline in N,N-dimethyl-formamide T=120°C; Rosenmund-von Braun reaction; 45 h;
参考文献
Wang, Deping; Kuang, Liping; Li, Zhengwei; Ding, Ke
Synlett, 2008 , # 1 p. 69 - 72
反应条件
in N,N-dimethyl-formamide T=120°C; Substitution; 16 h;
参考文献
Davis; Mohanty; Burns; Andemichael
Organic letters, 2000 , vol. 2, # 24 p. 3901 - 3903
反应条件
1: 1.) butyl-lithium / 1.) ether, hexane, -78 deg C, 1 h; 2.) ether, hexane, up to RT 2: 54 percent / aluminum chloride / chlorobenzene / 0.75 h / Heating View Scheme
参考文献
Evans, Geoffrey E.; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 755 - 762
反应条件
n-butyllithium in diethyl ether T=-15°C; 1 h;
参考文献
Griffin, David A.; Leeper, Finian J.; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 5 p. 1035 - 1042