hexamethylene tetramine hydrobromide perbromide in methanol; dichloromethane T=25 - 28°C; 0.25 h; Yield given. Yields of byproduct given;
参考文献
Smith, Keith; James, D. Martin; Matthews, Ian; Bye, Martin R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 15 p. 1877 - 1878
Huston; Hutchinson
Journal of the American Chemical Society, 1932 , vol. 54, p. 1504
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Huston; Peterson
Journal of the American Chemical Society, 1933 , vol. 55, p. 3879,3882
1: sodium dithionite; aqueous sodium carbonate 2: aqueous H2SO4 / Diazotization.Eintragen der Diazoniumsalz-Loesung in eine heisse Loesung von CuBr in wss. HBr unter gleichzeitigem Durchleiten von Wasserdampf 3: chloroform; bromine / Behandeln unter Kuehlung View Scheme
参考文献
Huston; Peterson
Journal of the American Chemical Society, 1933 , vol. 55, p. 3879,3882
1: aqueous H2SO4 / Diazotization.Eintragen der Diazoniumsalz-Loesung in eine heisse Loesung von CuBr in wss. HBr unter gleichzeitigem Durchleiten von Wasserdampf 2: chloroform; bromine / Behandeln unter Kuehlung View Scheme
参考文献
Huston; Peterson
Journal of the American Chemical Society, 1933 , vol. 55, p. 3879,3882