2-氯-4-硝基苯甲酸甲酯合成路线 (共 13 条)
反应条件
copper diacetate; acetic anhydride in N,N-dimethyl-formamide; acetonitrile T=130°C; 1 h; Sealed tube;
参考文献
European Journal of Organic Chemistry, , vol. 2014, # 10 p. 2027 - 2031
反应条件
N-chloro-succinimide; trifluorormethanesulfonic acid; palladium diacetate; N-fluoropyridinium trifluoromethanesulfonate in 1,2-dichloro-ethane T=100°C; 4 h; Sealed tube; regioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 16 p. 4440 - 4444
Angew. Chem., , vol. 125, # 16 p. 4536 - 4540,5
反应条件
copper quinolate in water; dimethyl sulfoxide T=120°C; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 78, # 19 p. 9898 - 9905
参考文献
Journal of the American Chemical Society, , vol. 71, p. 4154
反应条件
18-crown-6 ether; potassium carbonate T=90 - 150°C; 2 h;
参考文献
Synthetic Communications, , vol. 14, # 1 p. 77 - 82
参考文献
Journal of Medicinal Chemistry, , vol. 53, # 4 p. 1546 - 1562
反应条件
1: aqueous nitric acid / 120 - 180 °C 2: sulfuric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 4154
参考文献
Journal of the Chemical Society, , vol. 87, p. 1271
参考文献
Journal of the American Chemical Society, , vol. 71, p. 4154
反应条件
1: With ethanol; tin(ll) chloride T=0 - 90°C; 2: With sodium hydroxide in water; ethyl acetate
参考文献
Frantz, Marie-Celine; Rodrigo, Jordi; Boudier, Laure; Durroux, Thierry; Mouillac, Bernard; Hibert, Marcel
Journal of Medicinal Chemistry, 2010 , vol. 53, # 4 p. 1546 - 1562