2-氯-4-硝基苯甲酸甲酯合成路线 (共 13 条)
反应条件
tetrabutyl ammonium fluoride in dimethyl sulfoxide T=25°C; 0.166667 h; Inert atmosphereMicrowave irradiationAnhydrous conditions;
参考文献
LaBeaume, Paul; Placzek, Michael; Daniels, Mathew; Kendrick, Ian; Ng, Patrick; McNeel, Melissa; Afroze, Roushan; Alexander, Abigail; Thomas, Rhiannon; Kallmerten, Amy E.; Jones, Graham B.
Tetrahedron Letters, 2010 , vol. 51, # 14 p. 1906 - 1909
反应条件
1: With diisobutylaluminium hydride in hexane; dichloromethane T=-78°C; 4 h; Inert atmosphere; 2: With water in hexane; dichloromethane T=20°C; 0.333333 h; Inert atmosphere;
参考文献
CHLORION PHARMA, INC.; UNIVERSITE LAVAL; ATTARDO, Giorgio; TRIPATHY, Sasmita
Patent: WO2010/132999 A1, 2010 ;
Location in patent: Page/Page column 91 ;
反应条件
potassium carbonate; ethanethiol in water; acetone
参考文献
Stauffer Chemical Company
Patent: US4692545 A1, 1987 ;