暂无反应条件数据

1: methanol / 1.17 h / 70 °C 2: 5.5 g / NaBH4 / methanol / 1.17 h / 0 - 20 °C 3: 97 percent / 6 h / Heating 4: 35.5 percent / phenyliodine(III) diacetate / 0.67 h / 20 °C 5: 95 percent / BCl3 / CH2Cl2 / 20 h / -78 °C 6: 98 percent / pyridine / 1 h / 0 °C 7: 97 percent / formic acid; Et3N; PPh3 / Pd(OAc)2 / dimethylformamide / 3 h / 60 °C 8: 92 percent / pyridinium p-toluenesulfonate / benzene / 48 h / Heating 9: lithium aluminum hydride / tetrahydrofuran / 24 h 10: 20.6 mg / aq. HCl / tetrahydrofuran / 24 h / 20 °C View Scheme

selenium(IV) oxide; dihydrogen peroxide in tert-butyl alcohol T=20°C;

1: 2.47 g / 50percent aqueous KOH / methanol / 5 h / Heating 2: 1) thallium(III) nitrate / methanol / 1) 1 h, 2) 3 h 3: 190 mg / aqueous HCl / methanol / 4 h / Heating 4: 10 mg / concentrated HCl / acetic acid / 1 h / water-bath View Scheme