6-甲基-3(2H)-哒嗪酮合成路线 （共 28 条）
反应条件
bromine; acetic acid T=90°C; 6 h;
参考文献
Banerjee, Abhisek; Patil, Sandip; Pawar, Mahesh Y.; Gullapalli, Srinivas; Gupta, Praveen K.; Gandhi, Maulik N.; Bhateja, Deepak K.; Bajpai, Malini; Sangana, Ramachandra Rao; Gudi, Girish S.; Khairatkar-Joshi, Neelima; Gharat, Laxmikant A.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 19 p. 6286 - 6291
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in dichloromethane T=40°C; 24 h; Sealed tubeInert atmosphere;
参考文献
Donohoe, Timothy J.; Fishlock, Lisa P.; Basutto, Jose A.; Bower, John F.; Procopiou, Panayiotis A.; Thompson, Amber L.
Chemical Communications, 2009 , # 21 p. 3008 - 3010
反应条件
hydrogenchloride in ethanol 2 h; Heating;
参考文献
Baraldi; Bigoni; Cacciari; Caldari; Manfredini; Spalluto
Synthesis, 1994 , # 11 p. 1158 - 1162
反应条件
T=750°C; P=0.01 - 0.1 Torr; 1 h;
参考文献
McNab, Hamish; Stobie, Ian
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 8 p. 1845 - 1854
反应条件
BNO in benzene 3 h; Heating;
参考文献
Tetrahedron, , vol. 51, # 43 p. 11855 - 11862
反应条件
nitric acid T=160°C;
参考文献
Journal of the Chemical Society, , p. 2191,2194
反应条件
1: 88 percent / 99percent hydrazine hydrate / aq. ethanol / 2 h / Ambient temperature 2: 75 percent / 10percent HCl / aq. ethanol / 2 h / Heating View Scheme
参考文献
Synthesis, , # 11 p. 1158 - 1162
反应条件
1: 80 percent / molybdenum hexacarbonyl / acetonitrile; H2O / Heating 2: 88 percent / 99percent hydrazine hydrate / aq. ethanol / 2 h / Ambient temperature 3: 75 percent / 10percent HCl / aq. ethanol / 2 h / Heating View Scheme
参考文献
Synthesis, , # 11 p. 1158 - 1162
反应条件
1: hydrazine hydrate / ethanol / 3 h / |Reflux 2: bromine; acetic acid / 6 h / 90 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 19 p. 6286 - 6291
反应条件
in benzene 3 h; Heating;
参考文献
Tetrahedron, , vol. 51, # 43 p. 11855 - 11862
