6-甲基-3(2H)-哒嗪酮合成路线 （共 28 条）
反应条件
1: aqueous H2SO4 View Scheme
参考文献
Helvetica Chimica Acta, , vol. 37, p. 1467,1470
反应条件
2: NaNO2; acetic acid View Scheme
参考文献
Journal of the Chemical Society, , p. 239,242
反应条件
1: N2H4 2: NaNO2; acetic acid View Scheme
参考文献
Journal of the Chemical Society, , p. 239,242
参考文献
Helvetica Chimica Acta, , vol. 37, p. 1467,1470
反应条件
1: K2cr2O7 2: POCl3 View Scheme
参考文献
Homer et al.
Journal of the Chemical Society, 1948 , p. 2191,2194
反应条件
pyridine; tetraphosphorus decasulfide 2 h; Reflux;
参考文献
Nuss, Gernot; Saischek, Gerald; Harum, Bastian N.; Volpe, Manuel; Gatterer, Karl; Belaj, Ferdinand; Moesch-Zanetti, Nadia C.
Inorganic Chemistry, 2011 , vol. 50, # 5 p. 1991 - 2001
反应条件
potassium dichromate
参考文献
Homer et al.
Journal of the Chemical Society, 1948 , p. 2191,2194
Full Text Show Details
Libermann; Rouaix
Bulletin de la Societe Chimique de France, 1959 , p. 1793,1796
反应条件
1: K2Cr2O7 2: 52.5 percent / HCl / 14 h / Heating 3: 84.4 percent / POCl3 / 2 h / 100 °C View Scheme
参考文献
Morishita; Kobayashi; Yamada; Yajima
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 2 p. 371 - 372
反应条件
1: With phosphorus oxytribromide T=90°C; 1.5 h; Inert atmosphere; 2: With sodium hydrogencarbonate in water Cooling with ice;
参考文献
ABBOTT LABORATORIES; SCHRIMPF, Michael R.; LEE, Chih-Hung; LI, Tao; GFESSER, Gregory A.; MORTELL, Kathleen H.; FAGHIH, Ramin; NERSESIAN, Diana L.; SIPPY, Kevin B.; BUNNELLE, William H.; SCANIO, Marc; SHI, Lei; GOPALAKRISHNAN, Murali; DONNELLY-ROBERTS, Diana; HU, Min
Patent: WO2010/36998 A2, 2010 ;
Location in patent: Page/Page column 184 ;
反应条件
hydrazine hydrate T=150 - 160°C; 10 h;
参考文献
Gres'ko; Smolyar; Yutilov
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 7 p. 1026 - 1029
