in toluene
mixt. of Sb and Sn deriv. was allowed to stand in an evacuated glass ampoule at room temp. for 24 h; crystals of (p-Tol)4SbCl filtered off; filtrate evapd; residue chromd. on SiO2; identified by elem. anal.;
参考文献
Sharutin; Sharutina; Senchurin; Kovaleva; Shcherbakov; Gladyshev
Russian Journal of General Chemistry, 2000 , vol. 70, # 1 p. 64 - 65
in toluene
mixt. of Sb and Sn deriv. was allowed to stand in an evacuated glass ampoule at room temp. for 72 h; crystals of (p-Tol)4SbBr filtered off; filtrate evapd; residue chromd. on SiO2; identified by elem. anal. and NMR spectrum;
参考文献
Sharutin; Sharutina; Senchurin; Kovaleva; Shcherbakov; Gladyshev
Russian Journal of General Chemistry, 2000 , vol. 70, # 1 p. 64 - 65
in toluene
mixt. of equimolar amts. of Sb and Sn deriv. was allowed to stand in an evacuated glass ampoule at room temp. for 24 h; crystals of (p-Tol)4SbBr filtered off; filtrate evapd; residue chromd. on SiO2; identified by elem. anal.;
参考文献
Sharutin; Sharutina; Senchurin; Kovaleva; Shcherbakov; Gladyshev
Russian Journal of General Chemistry, 2000 , vol. 70, # 1 p. 64 - 65
in toluene
mixt. of Sb and Sn deriv. in a molar ratio 2:1 was allowed to stand in an evacuated glass ampoule at room temp. for 24 h; crystals of (p-Tol)4SbBr filtered off; filtrate evapd; residue chromd. on SiO2; identified by elem. anal. and NMR spectrum;
参考文献
Sharutin; Sharutina; Senchurin; Kovaleva; Shcherbakov; Gladyshev
Russian Journal of General Chemistry, 2000 , vol. 70, # 1 p. 64 - 65
→
反应条件
in diethyl ether
mixt. of (PhMe)5Sb and Bi sulfonate in ether kept for 48 h at 20°C; ppt. filtered, washed (hexane), dried; ethereal and hexane soln. evapd.,recrystd. from EtOH;
参考文献
Sharutin; Egorova; Pavlushkina; Ivanenko
Russian Journal of General Chemistry, 2002 , vol. 72, # 12 p. 1925 - 1926
