反应条件
1: tert-butyl 2-(1-vinylcyclohexyl)hydrazinecarboxylate With hydrogenchloride in dioxanes
24 h; Inert atmosphere;
2: With platinum(IV) oxide; hydrogen in methanol
48 h;
3: acetyl chloride With 4-(N,N-dimethlyamino)pyridine; triethylamine
Inert atmosphere;
参考文献
Strick, Benjamin F.; Mundal, Devon A.; Thomson, Regan J.
Journal of the American Chemical Society, 2011 , vol. 133, # 36 p. 14252 - 14255