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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘代苯乙酮
合成路线
（共 462 条）
106-44-5
对甲酚
+
13329-40-3
4-碘代苯乙酮
→
反应条件
71815-31-1
1-(4-(对甲苯氧基)苯基)乙酮
反应条件
tetrabutylammomium bromide; potassium carbonate in n-hexyl ether; dimethyl sulfoxide T=130°C; Ullmann reaction; 12 h; Open air atmosphere;
参考文献
Islam, Manirul; Mondal, Sanchita; Mondal, Paramita; Roy, Anupam Singha; Hossain, Dildar; Mobarak, Manir
Transition Metal Chemistry, 2011 , vol. 36, # 1 p. 1 - 11
13329-40-3
4-碘代苯乙酮
→
反应条件
71866-86-9
反应条件
1: 60 percent / SiCl4 / ethanol / 24 h / 20 °C 2: 97 percent / CuI; Pd(PPh3)2Cl2; PPh3 / Et3N / tetrahydrofuran / 5 h / 20 °C 3: 85 percent / K2CO3 / methanol; tetrahydrofuran / 3 h / 20 °C View Scheme
参考文献
Sirilaksanapong, Sakan; Sukwattanasinitt, Mongkol; Rashatasakhon, Paitoon
Chemical Communications, 2012 , vol. 48, # 2 p. 293 - 295
13329-40-3
4-碘代苯乙酮
+
1765-93-1
4-氟苯硼酸
→
反应条件
720-74-1
1-(4'-氟-4-联苯基)乙酮
反应条件
Pd(OH)2/Fe3O4; sodium carbonate in toluene T=130°C; Suzuki-Miyaura reaction; 24 h;
参考文献
Cano, Rafael; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 2011 , vol. 67, # 30 p. 5432 - 5436
13329-40-3
4-碘代苯乙酮
+
437-29-6
→
反应条件
720-74-1
1-(4'-氟-4-联苯基)乙酮
反应条件
potassium phosphate; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Banerjee, Debasis; Jadhav, Deepak N.
Tetrahedron Letters, 2007 , vol. 48, # 38 p. 6644 - 6647
13329-40-3
4-碘代苯乙酮
→
反应条件
720-74-1
1-(4'-氟-4-联苯基)乙酮
反应条件
N-ethyl-N,N-diisopropylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in water; isopropyl alcohol T=100°C; Suzuki coupling; 0.166667 h; microwave irradiation;
参考文献
Kabalka, George W.; Al-Masum, Mohammad
Tetrahedron Letters, 2005 , vol. 46, # 37 p. 6329 - 6331
13329-40-3
4-碘代苯乙酮
+
1066-54-2
三甲基乙炔基硅
→
反应条件
75883-03-3
反应条件
silver(l) oxide; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=60°C; 3 h;
参考文献
Mori, Atsunori; Kawashima, Jun; Shimada, Tomohiro; Suguro, Masahiro; Hirabayashi, Kazunori; Nishihara, Yasushi
Organic Letters, 2000 , vol. 2, # 19 p. 2935 - 2937
13329-40-3
4-碘代苯乙酮
→
反应条件
766-99-4
反应条件
1: trichlorophosphate 2: water; sodium hydroxide / 1,4-dioxane View Scheme
参考文献
Kotha, Sambasivarao; Seema, Vittal
Synlett, 2011 , # 16 art. no. D16111ST, p. 2329 - 2334
13329-40-3
4-碘代苯乙酮
+
26919-48-2
→
反应条件
76650-29-8
反应条件
potassium acetate; palladium diacetate; N,N-dicyclohexylamine in N,N-dimethyl-formamide T=35°C; 2 h; Inert atmosphere;
参考文献
Rao, Maddali L.N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Tetrahedron Letters, 2010 , vol. 51, # 47 p. 6101 - 6104
13329-40-3
4-碘代苯乙酮
+
107-13-1
→
反应条件
77120-12-8
反应条件
tributyl-amine in N,N-dimethyl-formamide T=120°C; Heck-Mizoroki reaction;
参考文献
Mennecke, Klaas; Solodenko, Wladimir; Kirschning, Andreas
Synthesis, 2008 , # 10 art. no. Z02308SS, p. 1589 - 1599
13329-40-3
4-碘代苯乙酮
+
201230-82-2
+
126485-51-6
→
反应条件
77976-03-5
+
127118-95-0
+
98-86-2
反应条件
potassium fluoride; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide P=760 Torr; 3 h; other arylfluorosilanes, other solvents, other catalysts, other temperatures, other pressures of CO, other products; Product distributionMechanism;
参考文献
Hatanaka, Yasuo; Hiyama, Tamejiro
Chemistry Letters, 1989 , p. 2049 - 2052
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