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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘代苯乙酮
合成路线
（共 462 条）
13329-40-3
4-碘代苯乙酮
+
16419-60-6
2-甲基苯硼酸
→
反应条件
56917-39-6
1-(2'-甲基[1,1'-联苯]-4-基)乙酮
反应条件
potassium fluoride; tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine in tetrahydrofuran T=20°C; Suzuki cross-coupling; 3 h;
参考文献
McNulty, James; Capretta, Alfredo; Wilson, Jeff; Dyck, Jeff; Adjabeng, George; Robertson, Al
Chemical Communications, 2002 , # 17 p. 1986 - 1987
13329-40-3
4-碘代苯乙酮
+
33872-80-9
邻甲苯基氯化镁
→
反应条件
56917-39-6
1-(2'-甲基[1,1'-联苯]-4-基)乙酮
反应条件
1: 2-methylphenylmagnesium chloride With zinc(II) chloride in 1-methyl-pyrrolidin-2-one; diethyl ether T=60°C; 0.333333 h; 2: 4'-iodoacetophenone With ((Cy2POH)2PdCl)2 in 1-methyl-pyrrolidin-2-one T=65°C; Negishi cross-coupling; 2 h; Further stages.;
参考文献
Xu, Hanhui; Ekoue-Kovi, Kekeli; Wolf, Christian
Journal of Organic Chemistry, 2008 , vol. 73, # 19 p. 7638 - 7650
13329-40-3
4-碘代苯乙酮
+
506-93-4
硝酸胍
→
反应条件
56923-83-2
反应条件
potassium phosphate; copper(l) iodide; N-methyl-glycine in acetonitrile T=70°C; Ullmann reaction; 10 h; Inert atmosphere;
参考文献
Xing, Hui; Zhang, Ye; Lai, Yisheng; Jiang, Yongwen; Ma, Dawei
Journal of Organic Chemistry, 2012 , vol. 77, # 12 p. 5449 - 5453
13329-40-3
4-碘代苯乙酮
+
112-55-0
十二硫醇
→
反应条件
56944-52-6
反应条件
anhydrous iron chloride; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=135°C; 24 h; Inert atmosphere;
参考文献
Wu, Jhih-Ru; Lin, Che-Hung; Lee, Chin-Fa
Chemical Communications, 2009 , # 29 p. 4450 - 4452
13329-40-3
4-碘代苯乙酮
+
552-16-9
邻硝基苯甲酸
→
反应条件
5730-96-1
1-(2'-硝基[1,1'-联苯]-4-基)乙烷-1-酮
反应条件
2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; N,N-dimethyl-aniline; silver carbonate; palladium dichloride T=150°C; 2 h;
参考文献
Wang, Zhiyong; Ding, Qiuping; He, Xiaodan; Wu, Jie
Tetrahedron, 2009 , vol. 65, # 24 p. 4635 - 4638
598-32-3
+
13329-40-3
4-碘代苯乙酮
→
反应条件
57918-94-2
反应条件
tetrabutyl-ammonium chloride; sodium hydrogencarbonate in N,N-dimethyl-formamide T=100°C; Heck Reaction; 5 h; Inert atmosphere; regioselective reaction;
参考文献
Huang, Yixiang; Wang, Pingping; Liu, Jiaqin; Cai, Mingzhong
Journal of Chemical Research, 2013 , vol. 37, # 6 p. 333 - 336
13329-40-3
4-碘代苯乙酮
+
78-94-4
→
反应条件
57918-94-2
+
115665-94-6
反应条件
triethylamine; palladium on activated charcoal in carbon dioxide T=80°C; P=75006 Torr; 60 h;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Gasparrini, Francesco; Villani, Claudio
Synlett, 1999 , # 3 p. 345 - 347
13329-40-3
4-碘代苯乙酮
+
100-47-0
→
反应条件
59211-64-2
反应条件
N,N,N',N,-tetramethylethylenediamine T=20°C; 5 h; UV-irradiation; Overall yield = 11 percent; Overall yield = 5 mg;
参考文献
Zheng, Xingliang; Yang, Luo; Du, Weiyuan; Ding, Aishun; Guo, Hao
Chemistry - An Asian Journal, 2014 , vol. 9, # 2 p. 439 - 442
13329-40-3
4-碘代苯乙酮
+
100-46-9
→
反应条件
59852-82-3
反应条件
potassium phosphate; ethylene glycol; copper(l) iodide in isopropyl alcohol T=80°C; 5 h;
参考文献
Yang, Chu-Ting; Fu, Yao; Huang, Yao-Bing; Yi, Jun; Guo, Qing-Xiang; Liu, Lei
Angewandte Chemie, International Edition, 2009 , vol. 48, # 40 p. 7398 - 7401
Angewandte Chemie, 2009 , vol. 121, # 40 p. 7534 - 7537
13329-40-3
4-碘代苯乙酮
+
927-74-2
→
反应条件
510754-35-5
反应条件
tris-(dibenzylideneacetone)dipalladium(0); K3PO4*7H2O in water; isopropyl alcohol T=80°C; Sonogashira coupling; 0.25 h; Under air;
参考文献
Liu, Chun; Bao, Fanying; Ni, Qijian
Arkivoc, 2011 , vol. 2011, # 11 p. 60 - 68
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