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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘代苯乙酮
合成路线
（共 462 条）
13329-40-3
4-碘代苯乙酮
+
927-74-2
3-丁炔-1-醇
→
反应条件
反应条件
1: With triethylamine; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=80°C; Sonogashira reaction; 2 h; 2: With hydrogenchloride T=20 - 30°C; 8 h;
参考文献
Pal, Manojit; Parasuraman, Karuppasamy; Gupta, Shalabh; Yeleswarapu, Koteswar Rao
Synlett, 2002 , # 12 p. 1976 - 1982
13329-40-3
4-碘代苯乙酮
→
反应条件
6326-64-3
反应条件
1: H3[PW12O40] / neat (no solvent) / 0.5 h / 90 °C / |Microwave irradiation 2: potassium carbonate / N,N-dimethyl-formamide; water / 0.5 h / 70 °C / |Green chemistry View Scheme
参考文献
Isfahani, Amir Landarani; Mohammadpoor-Baltork, Iraj; Mirkhani, Valiollah; Khosropour, Ahmad R.; Moghadam, Majid; Tangestaninejad, Shahram; Kia, Reza
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 5 p. 957 - 972
13329-40-3
4-碘代苯乙酮
+
98-80-6
苯硼酸
→
反应条件
6326-64-3
反应条件
1: potassium carbonate / N,N-dimethyl-formamide; water / 0.03 h / 70 °C / |Microwave irradiation; |Green chemistry 2: H3[PW12O40] / neat (no solvent) / 0.5 h / 90 °C / |Microwave irradiation View Scheme
参考文献
Isfahani, Amir Landarani; Mohammadpoor-Baltork, Iraj; Mirkhani, Valiollah; Khosropour, Ahmad R.; Moghadam, Majid; Tangestaninejad, Shahram; Kia, Reza
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 5 p. 957 - 972
13329-40-3
4-碘代苯乙酮
→
反应条件
6328-81-0
4-二苯甲基苯甲酸
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate; silver(l) oxide in diethyl ether T=60°C; Suzuki-Miyaura Coupling; 20 h; Inert atmosphereGloveboxSealed tube;
参考文献
Matthew, Smitha C.; Glasspoole, Ben W.; Eisenberger, Patrick; Crudden, Cathleen M.
Journal of the American Chemical Society, 2014 , vol. 136, # 16 p. 5828 - 5831
67-56-1
甲醇
+
13329-40-3
4-碘代苯乙酮
→
反应条件
63349-52-0
对碘苯乙酸甲酯
反应条件
[bis(acetoxy)iodo]benzene; sulfuric acid 1 h; Heating;
参考文献
Ni, Aiwu; France, Jessica E.; Davies, Huw M. L.
Journal of Organic Chemistry, 2006 , vol. 71, # 15 p. 5594 - 5598
14660-52-7
5-溴戊酸乙酯
+
13329-40-3
4-碘代苯乙酮
→
反应条件
6337-68-4
反应条件
1: 5-bromopentanoic acid ethyl ester With indium; copper(l) iodide; lithium chloride in tetrahydrofuran T=65°C; 12 h; 2: 4'-iodoacetophenone With tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl acetamide T=90°C; 24 h;
参考文献
Shen, Zhi-Liang; Goh, Kelvin Kau Kiat; Wong, Colin Hong An; Yang, Yong-Sheng; Lai, Yin-Chang; Cheong, Hao-Lun; Loh, Teck-Peng
Chemical Communications, 2011 , vol. 47, # 16 p. 4778 - 4780
3054-95-3
+
13329-40-3
4-碘代苯乙酮
→
反应条件
6337-70-8
反应条件
tributyl-amine; tetrabutyl-ammonium chloride; palladium diacetate in N,N-dimethyl-formamide T=90°C; 0.5 h;
参考文献
Battistuzzi, Gianfranco; Cacchi, Sandro; Fabrizi, Giancarlo; Bernini, Roberta
Synlett, 2003 , # 8 p. 1133 - 1136
539-74-2
+
13329-40-3
4-碘代苯乙酮
→
反应条件
6337-70-8
反应条件
1: 3-(bromo)propionic acid ethyl ester With indium; copper(l) iodide; lithium chloride in tetrahydrofuran T=65°C; 12 h; 2: 4'-iodoacetophenone With tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl acetamide T=90°C; 24 h;
参考文献
Shen, Zhi-Liang; Goh, Kelvin Kau Kiat; Wong, Colin Hong An; Yang, Yong-Sheng; Lai, Yin-Chang; Cheong, Hao-Lun; Loh, Teck-Peng
Chemical Communications, 2011 , vol. 47, # 16 p. 4778 - 4780
539-74-2
+
13329-40-3
4-碘代苯乙酮
→
反应条件
6337-70-8
反应条件
1: 3-(bromo)propionic acid ethyl ester With indium; copper(l) iodide; lithium chloride in tetrahydrofuran T=65°C; 12 h; 2: 4'-iodoacetophenone With bis-triphenylphosphine-palladium(II) chloride in 1-methyl-pyrrolidin-2-one T=70°C; 24 h;
参考文献
Shen, Zhi-Liang; Goh, Kelvin Kau Kiat; Wong, Colin Hong An; Yang, Yong-Sheng; Lai, Yin-Chang; Cheong, Hao-Lun; Loh, Teck-Peng
Chemical Communications, 2011 , vol. 47, # 16 p. 4778 - 4780
13329-40-3
4-碘代苯乙酮
→
反应条件
3814-20-8
反应条件
copper(l) iodide; thiourea; L-proline; sodium t-butanolate in dimethyl sulfoxide T=90°C; 24 h; Inert atmosphere;
参考文献
Qiao, Shu; Xie, Kun; Qi, Junsheng
Chinese Journal of Chemistry, 2010 , vol. 28, # 8 p. 1441 - 1443
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