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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘代苯乙酮
合成路线
（共 462 条）
13329-40-3
4-碘代苯乙酮
+
288321-56-2
→
反应条件
5359-04-6
对异丙烯基苯乙酮
反应条件
tetrabutyl ammonium fluoride; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=20°C; Alkylation; 1 h;
参考文献
Denmark, Scott E.; Wang, Zhigang
Synthesis, 2000 , # 7 p. 999 - 1003
13329-40-3
4-碘代苯乙酮
+
55-21-0
苯甲酰胺
→
反应条件
5411-13-2
N-(4-乙酰基苯基)苯甲酰胺
反应条件
caesium carbonate; bis[hydrotris(3-Me-imidazolin-2-ylidene)borate]triCu(I) BF4 in dimethyl sulfoxide T=100°C; 24 h;
参考文献
Tubaro, Cristina; Biffis, Andrea; Scattolin, Elena; Basato, Marino
Tetrahedron, 2008 , vol. 64, # 19 p. 4187 - 4195
13329-40-3
4-碘代苯乙酮
+
106-48-9
对氯苯酚
→
反应条件
41150-48-5
4-(4-氯苯氧基)苯乙酮
反应条件
(CuOTf)2.C6H6; naphthalene-1-carboxylic acid; caesium carbonate; ethyl acetate in toluene T=110°C;
参考文献
Marcoux; Doye; Buchwald
Journal of the American Chemical Society, 1997 , vol. 119, # 43 p. 10539 - 10540
13329-40-3
4-碘代苯乙酮
→
反应条件
5335-82-0
1,1'-(二硫代二-4,1-亚苯基)二-乙酮
反应条件
1,10-phenanthroline; CuCl2·2H2O; tetrabutyl ammonium fluoride; caesium carbonate; sulfur in water T=100°C; 24 h; Sealed tube;
参考文献
Li, Zhengkai; Ke, Fang; Deng, Hang; Xu, Hualong; Xiang, Haifeng; Zhou, Xiangge
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 18 p. 2943 - 2946
13329-40-3
4-碘代苯乙酮
+
1779-49-3
甲基三苯基溴化膦
→
反应条件
561023-21-0
反应条件
1: Methyltriphenylphosphonium bromide With n-butyllithium in tetrahydrofuran T=0°C; 2 h; 2: 4'-iodoacetophenone in tetrahydrofuran T=0 - 20°C; Wittig olefination;
参考文献
Li, Fu-Nan; Kim, Nam-Jung; Paek, Seung-Mann; Kwon, Do-Yeon; Min, Kyung Hoon; Jeong, Yeon-Su; Kim, Sun-Young; Park, Young-Ho; Kim, Hee-Doo; Park, Hyeung-Geun; Suh, Young-Ger
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 10 p. 3557 - 3567
13329-40-3
4-碘代苯乙酮
+
2065-66-9
甲基三苯基碘化膦
→
反应条件
561023-21-0
反应条件
potassium tert-butylate in tetrahydrofuran Wittig olefination;
参考文献
Ikeda, Hiroshi; Hoshi, Yosuke; Namai, Hayato; Tanaka, Futoshi; Goodman, Joshua L.; Mizuno, Kazuhiko
Chemistry - A European Journal, 2007 , vol. 13, # 33 p. 9207 - 9215
→
反应条件
5173-05-7
1-(1,1':2',1''-三联苯-4-基)乙酮
反应条件
Pd0(tris(tert-butyl)phosphine)2; water; caesium carbonate in ethylene glycol dimethyl ether T=80°C; Suzuki-Miyaura cross-coupling reaction; 22 h; Inert atmosphere;
参考文献
Yoshida, Hiroto; Okada, Kengo; Kawashima, Shota; Tanino, Kenji; Ohshita, Joji
Chemical Communications, 2010 , vol. 46, # 10 p. 1763 - 1765
13329-40-3
4-碘代苯乙酮
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
52807-17-7
1-(2-甲氧基苯基)-3-甲基哌嗪
反应条件
Cyphos® IL 101; potassium phosphate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in toluene T=50°C; Suzuki cross-coupling; 1 h;
参考文献
McNulty, James; Capretta, Alfredo; Wilson, Jeff; Dyck, Jeff; Adjabeng, George; Robertson, Al
Chemical Communications, 2002 , # 17 p. 1986 - 1987
13329-40-3
4-碘代苯乙酮
+
83724-41-8
三(2-甲氧苯基)铋
→
反应条件
52807-17-7
1-(2-甲氧基苯基)-3-甲基哌嗪
反应条件
1,4-diaza-bicyclo[2.2.2]octane; Na3PO4*12H2O; 10 Pd/C in 1-methyl-pyrrolidin-2-one T=120°C; 24 h; Inert atmosphere;
参考文献
Monguchi, Yasunari; Hattori, Tomohiro; Miyamoto, Yasuhiro; Yanase, Takayoshi; Sawama, Yoshinari; Sajiki, Hironao
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 13 p. 2561 - 2567
13329-40-3
4-碘代苯乙酮
+
100-66-3
苯甲醚
→
反应条件
13021-18-6
1-(4-甲氧基-联苯-4-基)-乙酮
+
52807-17-7
1-(2-甲氧基苯基)-3-甲基哌嗪
+
76650-30-1
1-(3'-甲氧基联苯-4-基)乙酮
反应条件
N,N,N',N,-tetramethylethylenediamine T=20°C; 16 h; UV-irradiation; Overall yield = 94 percent; Overall yield = 43 mg;
参考文献
Zheng, Xingliang; Yang, Luo; Du, Weiyuan; Ding, Aishun; Guo, Hao
Chemistry - An Asian Journal, 2014 , vol. 9, # 2 p. 439 - 442
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