1: 1,1,1-trifluoro-2-chloroethane With zinc(II) chloride in tetrahydrofuran T=20°C; 2 h; 2: 4'-iodoacetophenone With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=65°C; 3 h; Title compound not separated from byproducts;
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Anilkumar; Burton, Donald J.
Journal of Fluorine Chemistry, 2005 , vol. 126, # 5 p. 835 - 843
Hirabayashi, Kazunori; Kondo, Tatsuhiro; Toriyama, Fumihiko; Nishihara, Yasushi; Mori, Atsunori
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 3 p. 749 - 750
1: 4'-iodoacetophenone With lithium chloride in N,N-dimethyl-formamide T=80°C; 2: 1-(iodo)-4-methylbenzene With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in N,N-dimethyl-formamide T=80°C; 3 h; Inert atmosphere;
参考文献
Papoian, Vardan; Minehan, Thomas
Journal of Organic Chemistry, 2008 , vol. 73, # 18 p. 7376 - 7379